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- Give examples of sample analyte in a matrix.How does it affect the peak produced in gas chromatography when: – Inserting samples is too slow – Column temperature is too hightwo chromatograms after LC separation. Which chromatogram is better to proceed for MS analysis? What mobile phase condition/composition (LC separation) was used?
- Retention time is the time taken for the mobile phase to reach the detector. True Falsecalculate the following for each sample gas chromatograph. a) retention time for each peak (label peaks) b) area of each peak c) %composition Sample GC of starting material for distillation of solution that is 40% ethyl acetate and 60% propyl acetate.Explain why a chromatographic separation normally has an optimum flow rate that gives the best separation.
- Which components in a liquid chromatography (LC) instrument are similar to the experimental set-up?the efficiency of a chromatographic column improves the measure thata.increases the height of the theoretical dishesb.decreases the number of theoretical platesc.platform height is reducedd.None of the above Please explain it Provide clear handwriting and clear imageThe plot of retention time versus detector signal in chromatography called?