Consider a crystallization of sulfanilamide in which 10mL of hot 95% ethyl alcohol is added to 0.10 g of impure sulfanilamide. After the solid has dissolved, the solution is cooled to room temperature and then placed in an ice-water bath. No crystals form, even after scratching with a glass rod. Explain why this crystallization failed. What would you have to do at this point to make the crystallization work? Assume that starting over again with a new sample is not an option.
Consider a crystallization of sulfanilamide in which 10mL of hot 95% ethyl alcohol is added to 0.10 g of impure sulfanilamide. After the solid has dissolved, the solution is cooled to room temperature and then placed in an ice-water bath. No crystals form, even after scratching with a glass rod. Explain why this crystallization failed. What would you have to do at this point to make the crystallization work? Assume that starting over again with a new sample is not an option.
Chapter2: Crystallization
Section: Chapter Questions
Problem 1Q
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Consider a crystallization of sulfanilamide in which 10mL of hot 95% ethyl alcohol is added to 0.10 g of impure sulfanilamide. After the solid has dissolved, the solution is cooled to room temperature and then placed in an ice-water bath. No crystals form, even after scratching with a glass rod. Explain why this crystallization failed. What would you have to do at this point to make the crystallization work? Assume that starting over again with a new sample is not an option.
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