Determine the structure of this NMR spectrum Provide the chemical shift, splitting pattern of signal

Organic Chemistry
9th Edition
ISBN:9781305080485
Author:John E. McMurry
Publisher:John E. McMurry
Chapter13: Structure Determination: Nuclear Magnetic Resonance Spectroscopy
Section13.SE: Something Extra
Problem 66GP: A 13C NMR spectrum of commercially available 2,4-pentanediol, shows five peaks at 23.3, 23.9, 46.5,...
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Determine the structure of this NMR spectrum Provide the chemical shift, splitting pattern of signal
p-BROMONITROBENZENE
13C NMR SPECTRUM
Solvent: Chloroform-d
'C NMR you
se for your
it
170
160
150
140
130
120
110
100
90
80
70
60
50
40
30
20
10
ppm
–147,10
-132.72
130.09
-125.11
Transcribed Image Text:p-BROMONITROBENZENE 13C NMR SPECTRUM Solvent: Chloroform-d 'C NMR you se for your it 170 160 150 140 130 120 110 100 90 80 70 60 50 40 30 20 10 ppm –147,10 -132.72 130.09 -125.11
p-BROMONI TROBENZENE
1H NMR SPECTRUM
Expansion of the 7.2-8.5 ppm region
Solvent:Chloroform-d
IR spectrum
se for your
8.4
8.3
8.2
8.1
8.0
7.9
7.8
7.7
7.6
7.5
7.4
ppm
9.5
9.0
8.5
8.0
7.5
7.0
6.5
6.0
5.5
5.0
4.5
4.0
3.5
3.0
2.5
2.0
1.5
1.0
0.5
ppm
-8.117
660 8
.704
-8.117
660'8S
704
989.
Transcribed Image Text:p-BROMONI TROBENZENE 1H NMR SPECTRUM Expansion of the 7.2-8.5 ppm region Solvent:Chloroform-d IR spectrum se for your 8.4 8.3 8.2 8.1 8.0 7.9 7.8 7.7 7.6 7.5 7.4 ppm 9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 ppm -8.117 660 8 .704 -8.117 660'8S 704 989.
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