Drye quantity of primary standard potassim hydrogen phthalate (CHP) for about 2 heat 110°C (Fig. 35-9), and cool in a desiccator. Weigh individual 0,7 to 0.8 g somples (to the nearest 0.Img) into 250 mi conical flasks, and dissolve each in 50 to 75 mL of distilled water. Add 2 drops of phenolphthalein; titrate with base until the pink colour of the indicator persists for 30 seconds (Note). Calculate the concentration of the NaOH solution.
Q: A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted…
A: The balanced chemical reactions are as follows: I- + OCl- + H2O = I2 + Cl- + 2OH- 2 Na2S2O3 + I2 =…
Q: An acid solution containing 2 per cent by mass of NaNO3, and an unknown concentration of HNO3 is…
A:
Q: One litre of aqueous sample containing the organic pollutant, polychlorinated biphenyl (PCB), was…
A: A one litre sample of polychlorinated biphenyl sample is extracted with two times each time with 50…
Q: Vhich of the followings is the important feature for choosing a good solvent for any…
A: Recrystallization is the method of purification of solute where the compound of interest is first…
Q: Using the given TLC plate can you describe the results and what does the TCL plate tell about the…
A: To describe the results on TLC plate for purity.
Q: You are required to prepare working standard solutions of 1.00 × 10−5, 2.00 × 10−5, 5.00 × 10−5, and…
A: Given M₁ = 0.100M stock solution V₁ = volume of Stock solution M₂ = Working standard V₂ = Volume of…
Q: -why HCI is not primary standard material ? -It is usually impossible to obtain NaOH of sufficient…
A: To be a primary standard it's concentration must be known exactly. They should not interact with…
Q: What are the principles behind caffeine being extracted from coffee using the above items?
A: Caffeine extraction from coffee
Q: lews SEC # Evaluation of Commercial Bleaching Solutions 22 DATA SHEET Brand name of commercial…
A: Concentration of NaOCl = M1 = 0.175M VOlume of NaOCl = V1 Concentration of KI = M2 = 0.225M Volume…
Q: A large volume of liquid is found to have some insoluble solid present in the bottom of the…
A: Various techniques has been used for the purification of the substances.
Q: How many ml of 0.241 M Ba(OH)2 will react with 25.00 mL of 0.115 М НCI?
A: This is an example of acid-base reaction. Ba(OH)2 + HCl -------> BaCl2 + H2O
Q: 6. If more polar impurities are desired to be eluted first and then analyte, then at which stage do…
A: 6. If more polar impurities are desired to be eluted first and then analyte, then at step (c) i.e.…
Q: To determine the soil distribution coefficient (Kd), 10 g of dry soil is spiked with 100 mg of…
A: The distribution coefficient Kd can be calculated using the expression: Kd=Atrazine present in…
Q: An environmental chemist working for the Environmental Protection Agency (EPA) was directed to…
A: Varying amounts of 85.0 ppb (μg/L) Cd2+ standard solution were added to the unknown sample solution.…
Q: Melting point: 122-123 experimental product melting point: 120 mass of starting material: 1.04…
A: A numerical problem based on yield, which is to be accomplished.
Q: Accurately prepare a 50cm stock solution of (approx.) 0.003M potassium permanganate solutic Very…
A: Given that: the volume of potassium permanganate solution = 50 cm3 the volume of potassium…
Q: 1. What is the difference between distribution coefficient and distribution ratio? 2 How does SPE…
A: Since we only answer up to 3 sub-parts, we’ll answer the first3. Please resubmit the question and…
Q: Methodology: Make schematic diagram for the procedure below B. % SO3 determination Dry the soluble…
A: We need to make a schematic diagram for the given procedure.
Q: and in 4) To adjust the thiosulfate (S2O32) solution to be used as a titrant in the copper…
A:
Q: A flavor chemist attempted to isolate and identify the major flavor component of a recently…
A: IR : 3100 cm-1 sp2 C-H stretch, 2950 cm-1 sp3 C-H stretch, 1735 cm-1 carbonyl stretch of ester, 800…
Q: A three-component mixture containing AgCl, SiO2, and KBr was provided to you in the lab to isolate.…
A: Filtration is a separation technique which is used for the separation of an insoluble salt from a…
Q: A 2.067 g of macrogol monostearate (average molecular weight 706. 5) was added to a 200 ml flask and…
A: Solution: We know the macrogol monostearate is the ester of stearic acid. Saponification is the…
Q: After the extraction of benzoic acid from 0.5g impure sample, the weight of pure benzoic acid in the…
A: The given data- The weight of the impure sample = 0.5 g The weight of the pure benzoic acid = 0.4 g…
Q: Which of the following could DECREASE the amount of the recovered crystals in the purification by…
A:
Q: 6. The following are disadvantages of using filter paper in gravimetry, which is not included? а.…
A: 6) c is the correct answer. IN the Gravimetry we uses the ashless filter paper to achieve the…
Q: 0.56 g 1,4‐dimethoxybenzene, 0.9 mL 2‐chloro‐2‐methylpropane, 5 mL nitrobenzene and 0.52 g graphite…
A: The given problem is related to green chemistry. Given: Reactants- Mass of 1,4‐dimethoxybenzene-…
Q: A 5.00 ml sample of white vinegar is diluted in acetone and analyzed by GC-TCD using 1-propanol as…
A: Given options,
Q: A brewed tea brand sample was subjected to solvent extraction to extract caffeine. The cup of tea…
A:
Q: • If the unknown is vinegar (Note 1), pipet 25.00 mL into a 250 mL volumetric flask and dilute to…
A: This is acid base titration using phenolphthalein indicator. Vinegar is chemically acetic acid.
Q: I just need help figuring out the values to do a calculation. Part of the lab relevant... "Prepare…
A: Phosphate ion can be determined by using the method called ascorbic acid method or molybdenum blue…
Q: A weight of 0.50 g was taken impure container containing sodium carbonate and bicarbonate. Dissolved…
A: In the carbonate composition analysis, the mixture containing unknown amounts of sodium carbonate…
Q: Fill out the Flow Scheme below. Obtain your ternary mixture and follow the steps on p. 2. in CH,Cl2…
A: 3 compounds need to be extracted. Benzoic acid Ethyl – p - aminobenzoate Naphthalene in…
Q: B. %SO3 determination 1. Dry the soluble sulfate sample at 100°C for 1-2 hours, and cool in…
A: We need to make a schematic diagram for the given procedure.
Q: crucible and precipitate are dry?
A: For precipitate are dry: Pour the methanol into the crucible ,swirl gently ,…
Q: Anion Test - Sulfate (SO42-) Procedure : Mix 5 drops of SO42- (Na2SO4 0.5 M) with 5 drops of HCl…
A: Answer: Sulfate test: Barium chloride (BaCl2) is used to detect the sulfate anion (SO42-) in aqeous…
Q: Please provide explanation 1. Which of the following techniques help prevent premature…
A: As per the guideline, since you have asked multiple questions, we have solved the first question for…
Q: burned in pure 02 and the combustion gases collected in absorbent tubes. The tube used to trap CO2…
A: Ans. The conservation of mass requires that all the carbon in the organic compound must be in the…
Q: RECRYSTAI PTIONAL 1. Begin assembling your reflux apparatus (i.e. lab jack, stir plate, exten- sion…
A: Recrystallization is a process use to purify the impure product by dissolving in appropriate…
Q: Which of the following could result in a loss in yield in a mixed solvent recrystallization? i. Use…
A:
Q: A 5.00 mL sample of white vinegar is diluted in acetone and analyzed by GC-TCD using 1-propanol as…
A:
Q: why is it necessary to test the ph? EXTRME DETAIL PLEASE PROCEDURE To a six inch test tube was…
A: Please find your solution below : Benzoin condensation is an addition reaction between two aldehydes…
Q: or each item, explain in one (1) sentence why the step is done in the gravimetric analysis of…
A:
Q: Please help me there are multiple parts, double check your answer as previous tutors got it wrong.
A: The given illustration is the procedures for the preparation of borax solution.
Q: Indicate with (+) or (-) if the test compound is soluble or insoluble in the solvent. Is Acetanilide…
A: Solubility of organic compound depend on the nature of functional group present
Q: Upon this addition of potassium chromate, you observe no formation of precipitate. Which of the…
A: Pb2+, Ag+, and Hg22+ give a white precipitate with HCl. So the formation of white precipitate with…
Q: Mud filtration test to determine volume of filtrate and the ermeability of mud cake collected after…
A: Given that Permeability of mud cake collected after 30 min
Q: Data Sheet with Sample Results Note: results that require calculations are purposely left blank and…
A: (7) Mass of NaCl dissolved : Mass of NaCl dissolved = (Mass of 50mL beaker + Stirring bar + NaCl) -…
Q: in ethyl acetate (organic) treat with aqueous HCI Aqueous layer Organic layer treat with treat with…
A:
Q: set-up, e volatile acetc е аcet
A: Given data set: Mass of the empty flask = 351.44 g Mass of the heated flask = 355.02 g Thus, Mass of…
Q: nion Test - Iodide (I-) Procedure : Dilute 6 drops of I- solution (NaI 0.5 M) by 12 drops of…
A: Double displacement (Metathesis) When the anions and cations of two different molecules switch…
Step by step
Solved in 9 steps
- After the extraction of benzoic acid from 0.5g impure sample, the weight of pure benzoic acid in the filter paper was 0.4g. Calculate the % impurity?from this pfd of nitrobenzene production show material balance at mixing -the conversion is 99% and production 1000 ton/day1.063 g of p-acetamidophenol was measured out into a 50 mL round bottom flask along with 8 mL of 1M NaOH in ethanol and a stir bar. This mixture was heated at reflux for 15 min. It was allowed to cool and then 0.80 mL of bromoethane was added to the reaction. The mixture was then heated at reflux for another 15 min. After heating, the solution was poured onto a mixture of ice and water and further cooled on ice and then the solid was collected by vacuum filtration. This solid was then recrystallized from ethanol and water. The final mass of the purified phenacetin was 0.42250 g and it had a melting point of 127 - 130 C. The TLC plate shows (from left to right) pure p-acetamidophenol, the reaction mixture before pouring it on ice/water, phenacetin after recrystallization. The solvent used was a mixture of 80% ethyl acetate and 20% heptane with 0.5% acetic acid added. QUESTION: Using the given TLC plate can you describe the results and what does the TCL plate tell about the purity?
- For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 1. Na2CO3 is often added to thiosulfate…For Indirect Iodometric Analysis of Copper... ~0.0896g KIO3 necessary to consume 350mL of 0.1 M Na2S2O3, Na2S2O3 is stored in an amber glass bottle until ready for use. Primary Standard KIO3 has 2g of KI, 50mL of DI water, and 10 mL of 1.0M HCl is added then immediately titrated with Na2S2O3 until medium yellow or straw... then 5mL of starch indicator is added and titrated again until blue black color turns clear. Unknown CuO use 1.2G of Unknown, 20mL of HNO3 heated until sample dissolved, 25 mL of DI water added and boiled until clear light blue color, after cooling 1:1 NH3 added (~34.47 mL of NH4OH reagent) until permanent deep blue color amine complex, 2g of NH4HF2 added and swirled until dissolved, 3 g of KI is added then titrated immediately with Na2S2O3 until brown color of iodide is nearly gone (brown milk color), 2 g of KSCN and 3 mL of starch indicator is then added with titration continuing until disappearance of new blue black color. 4. Why is the starch indicator solution…0.56 g 1,4‐dimethoxybenzene, 0.9 mL 2‐chloro‐2‐methylpropane, 5 mL nitrobenzene and 0.52 g graphite were combined, and the mixture was refluxed for 1.5 hours. It was then cooled to room temperature and filtered. The filtered graphite was washed with 15 mL hexane. The filtrate was distilled under vacuum to remove any remaining 1,4‐dimethoxybenzene, 2‐chloro‐2‐ methylpropane and nitrobenzene (6.3 g), yielding 0.44 g 1,4‐di‐tert‐butyl‐2,5‐dimethoxybenzene (43.4% yield). What is the Atom economy, E factor, and effective mass yield?
- I just need help figuring out the values to do a calculation. Part of the lab relevant... "Prepare standards on the same day they will be used. Using a 100 mL volumetric flask, add x mL (vide infra) of the 0.050 mg/mL phosphate standard, 20 mL of th e molybdate-antimoney reagent, 1 mL of ascorbic acid, and dilute to volume with ultrapure water. Do this procedure for x = 0 mL, 1 ml, 2 ml, 5 ml, and 10 ml using volumetric pipettes. To be clear, we will be making 5 different solutions. The equation that was given was Concentration of initial standard (mg/mL) multiplied by volume added (mL) = concentration of created standard multiplied by volume of volumetric I dont need you to do the calculations, I just need help finding what values go in equation. we are trying to find the concentration of created standardSuppose you have a soil that is made up of 10% organic matter with CEC = 200 cmol/kg, 40% kaolinitewith CEC = 10 cmol/kg, and 50% vermiculite with CEC = 100 cmol/kg.1- Calculate the overall CEC of the soil by taking a weighted average of the three soil components.2- What percentage of the overall CEC is contributed by the organic matter? How does that numbercompare to the 10% of the soil itself that is organic?Prior to fat analysis, two samples: Sample 1 and Sample 2 with the initial weight for each sample=2.50g. After pre-dried, samples were grinded and reweighted; s1-2.15g and s2=2.11g. Samples were placed in dried glass wool in each thimble and placed extractor for 4-5 hours. Samples were then dried and cooled in desiccators before another weight recorded. The weight for s1=93.51g and for s2=93.78g #Weight of round bottom flask (with glass wool+ thimble) (g) = 92.00 #Weight of round bottom flask (g) =91.00 1) Calculate the percentage of dried fat in s1 2) Calculate the percentage of dried fat in s2. 3) Sample 3 have dried fats of 50%. Identify the correct sequence from the highest to the lowest % of dried fats in sample.
- Volume of acetic anhydride: 2.98 mL Mass of salicylic acid: 1.00 g Mass of aspirin recovered: 0.67 g Show that mmol of aspirin recovered divided by mmol of limiting reagent x 100% gives the same % yield (please explain) Thank you.The concentration of purified OXA-M290 is tested with a BCA assay. Serial dilutions of a bovine serum albumin (BSA) stock solution are prepared, then pipetted into a 96-well plate; each dilution of the BSA standard is tested in triplicate. Then, bicinchoninic acid and Cu2+ ions are added to all of the wells of the plate. After incubating the plate for 1 hour, a microplate reader is used to measure the absorbance of all of the wells in the plate at 560 nm. This generates the following data: BSA conc. (μg/mL), Replicate 1 Absorbance, Replicate 2 Absorbance, Replicate 3 Absorbance 40, 1.360, 1.403, 1.481 20, 0.750, 0.745, 0.810 10, 0.380, 0.344, 0.398 5, 0.198, 0.160, 0.183 2.5, 0.090, 0.100, 0.085 1.25, 0.038, 0.043, 0.051 0.625, 0.024, 0.028, 0.019 Prepare a calibration curve using these data. You can use Excel, R, SPSS or an equivalent graphing software. In this graph, plot absorbance (y-axis) against the concentration of the protein standard (x-axis). Calculate and plot…A sample of anhydrous Na2CO3 (FM = 105.989) is suspected to be contaminated with eitherNaHCO3 (FM = 84.007) or NaOH (FM = 39.997) To verify the suspicion, a 0.7483 g sample was dissolved to prepare a 50.00 mL solution, and a 10.00 mL aliquot was taken to prepare a 100 mL solution, where 25.00 mL was analyzed using single flask method. If the sample requires 27.50 mL of standard 0.0125 N HCl to reach the phenolphthalein endpoint and another 28.40 mL to reach the bromcresol green endpoint, calculate the percentagecomposition (in %w/w) of all the basic components in the sample.