Ex(1): In the analysis for chloride. The sample weighed (0.8732 gm) and the AgCI (p.p.t) from the sample weighed (1.0292 gm). Calculate the precent of chloride in the sample. At. wt. of Cl= 35.5, Ag = 101.88.
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- 00 mL of a diprotic acid primary standard solution was accurately prepared to a concentration of 0.1431 M. Three samples of this primary standard solution were used as samples in a titration to standardize an aqueous solution of sodium hydroxide, NaOH, which would be used as a titrant. Using the following table of data for the titration of the primary standard acid with NaOH, calculate the average concentration of NaOH. Trial # Volume of primary standard Initial titrant volume Final titrant volume 1 10.00 mL 8.21 mL 27.22 mL 2 10.00 mL 27.22 mL 46.23 mL 3 10.00 mL 30.28 mL 49.29 mL 0.1506 M 0.0753 M 0.0376 M 0.1431 M 0.0526 MA 50 mL sample solution containing 8-hydroxyquinoline (MW: 145) was analyzed by adding 25 ml, 0.1 M KBrO3, excess KBr and acidified. The mixture was left for 10 minutes in dark place. After this time KI in excess was added followed by titration with 27.9 mL, 0.05 M thiosulfate standard solution. Write balance equations? What is the percent w/v 8-hydroxyquinoline in sample?A sodium thiosulfate solution can be standardized by using it to titrate the iodine liberated by the action of excess KI on a known weight of primary standard K2Cr2O7: Cr2O72- + 6I- + 14H+ → 2 Cr3+ + 3I2 + 7H2O I2 + 2S2O32- → 2I- + S4O62- Calculate the molar concentration of the sodium thiosulfate solution if 31.47 mL of this solution were required to titrate a sample prepared using 0.2177 g pure K2Cr2O7.
- Compare and contrast an anticipatory standard to a reactionary standard by listing and describing some advantages and disadvantages.Calculate the gravimetric factor of the following. 2 Fe is sought(Analyte), 1Fe2O3 is weighed (Precipitate)Make an schematic diagram for procedure below: B. %SO3 determination Transfer all precipitate to the filter paper avoiding any loses during the filtration procedure. One may use a rubber policeman to scrape remaining precipitate in the beaker. Wash the precipitate in the beaker 3x with hot water before transferring to the filter paper. Test the washings with 0.1 M AgNO3 Cloudiness indicates presence of chloride ions; therefore there is a need to wash more the precipitate. Carefully lift the paper out of the funnel, fold it as demonstrated by your instructor and transfer it onto the constant weighed crucible. Dry the crucible cautiously with a small flam, as instructed by your instructor. The flame should be directed at the top of the container, and the lid should be off. Avoid spattering. After drying, char the filter paper by increasing the flame temperature. The crucible should have free access to air. The lid should be kept handy to smother the filter paper in case it catches fire.…
- The student then determined ΔH neutralization for the reaction of sodium hydroxide and acetic acid, using the procedure described in this module. The student added 100.0 mL of 0.8500M NaOH to 100.0 mL of 0.8404M acetic acid. Prior to and following the mixing of the acid and base solutions, the following temperature-time data were collected. g) Identify the limiting reagent and briefly explain why it is limiting. h) Find ΔH neutralization for the reaction.Hexanoic acid was added to an immiscible biphasic solvent sysem, water and CCl4 at 20.0OC and the equilibrium concentrations of hexanoic acid were determined to be 3.66 g/L in H2O and 67.0 g/L in CCl4. Caluclate the distrubution coeffiecent (D1) of hexanoic acid in CCl4 with respect to water.A pH probe/meter uses the following equations: Ecell = L + 0.0592 log a1 = L - 0.0592 pH Where L = L1 + EAg/AgCI + Easy= constants L1 = - 0.0592 log a2 a1 = activity of analyte solution a2 = activity of internal solution Questions: How will measured pH value be affected vs “real” pH if the temperature of the sample is 30C when pH was measured? How will measured pH value be affected vs “real” pH if HCl in pH electrode, became 0.15M instead of 0.1M? How pH value will be affected vs “real” pH if the glass of the pH electrode is not fully hydrated? Please answer all questions and provide a brief explanation
- -Please determine the ksp for Cu(OH)2. pH for solution was 5.25 Show ice box for chemical equation. please show all steps to solution clearlyIn gravimetric analysis, co-precipitation occurs alongside with analyte precipitation,resulting in the introduction of impurity and excess mass. Occlusion and inclusion areamong the sources of impurities. Distinguish the difference between occlusion andinclusion and compare them using diagramsSources of Error Determine the relationship between the observed/apparent value (EX) VERSUS that of the true value (ET) for the quantity being sought by writing either <, >, or = on the space provided. TOPIC: Measured mass of the precipitate 1. Overignition which causes the conversion of BaSO4 precipitate to BaO. EX _____ ET2. Precipitate was not washed thoroughly. Ex _____ ET TOPIC: Standardization of Titrant 3.Distilled water was not equilibrated to room temperature before the preparation of NaOH titrant. EX _______ ET
