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a primary standard of (COOK)2.H2O was prepared up to 0.05M. This primary standard was then titred against an unknown concentration of 50cm3 of KMnO4. An average titre value of 13 was obtained. The balanced equation is as follows:
5(COOK)2.H2O + 2KMnO4 + 8H2SO4 = 6K2SO4 +2MnSO4 + 10CO2 +18H2O.
Find the concentration of the KMnO4.
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- A 0.1093-g sample of impure Na2CO3 was analyzed by the Volhard method. After adding 50.00 mL of 0.06911 M AgNO3, the sample was back-titrated with 0.05781 M KSCN, requiring 27.36 mL to reach the endpoint. Report the purity of the Na2CO3 sample. [Ans. 90.9 % (w /w )]1. 1093-g sample of impure Na2CO3 was analyzed by residual precipitimetry. After adding 50.00 mL of 0.06911 M AgNO3, the sample was back-titrated with 0.05781 M KSCN, requiring 27.36 mL to reach the endpoint. The percentage Na2CO3 (MW = 106.0 g/mole) in the tested sample is ________ % ? Note: Express final answer using least number of significant figures. 2. The alkalinity of natural waters is usually controlled by OH- (MW = 17.01 g/mole), CO3-2 (MW = 60.01 g/mole), and HCO3- (MW = 61.01 g/mole), which may be present singularly or in combination. Titrating a 10.0-mL sample to a phenolphthalein endpoint requires 38.12 mL of a 0.5812 M solution of HCl, and an additional 18.67 mL of the same titrant to reach the methyl orange endpoint. The composition of the sample is _________% CO3-2 and ___________ % OH- Note: Express final answers using least number of significant figures.Mr. Clean recently bought a laboratory-grade sodium carbonate from a chemical company known as Brand X. He was supposed to use it in the production of detergents. Unfortunately, he was scammed by the company. He suspected that he purchased a crude sodium carbonate so he tasked the Quality Assurance Department to determine the components of the purchased chemical. The chemist assigned to analyze the sample used double indicator method. For the standardization of HCl titrant, 0.1025 g Na2CO3 of 99.5% purity (FW: 106.00) required 8.20 mL of the titrant to reach the phenolphthalein endpoint. FW: NaOH (40.00), NaHCO3 (84.01), Na2CO3 (106.00) a. What is the molarity of the titrant? The chemist obtained a 3.150 g sample and dissolved it in distilled water to produce a 50.0 mL solution. An aliquot of 10.00 mL was obtained and diluted in a 100.0 mL volumetric flask. A 50.00-mL aliquot of the diluted sample was taken and it required 25.70 mL of titrant for the methyl orange endpoint, while…
- A deep well sample of 100 mL was titrated with 0.010 M EDTA at pH=10 (with Mg-EDTA-pH 10 reagent) and consumed 30.15 mL using EBT indicator. Titration of another 100 mL of the same deep well sample with same titrant but the pH was adjusted to 12.10 and murrexide as indicator consumed 24.25 to reach end point. Calculate: a. Total hardness of water as CaCO3 b. ppm of Ca and MgThe buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of solubility and Ksp of calcium hydroxide: Trial 1: Final Buret reading (ml)-19.80; Initial Buret reading (ml)- 13.00; Temperature (Celcius)- 25 Trial 2: Final Buret reading (ml)-26.10; Initial Buret reading (ml)- 19.80; Temperature (Celcius)- 25 Voume of HCl used: Trial 1- 6.80ml; Trial 2- 6.30mL 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Construct an ICE table for the reaction.3. Calculate the molar solubility (in mol/L) of OH- and Ca2+.4. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 5.…Calcium fluoride is considered as a relatively insoluble compound and therefore lime or slakedlime has been considered as a possible material to remove excess fluoride in water of boreholesin certain parts of the country. The solubility product of CaF2 is Ksp = 3 x 10 – 11 and that ofCa(OH)2 isKsp =8x10-61. How much lime can be added to the water to remove 10 mg of F- ion per litre ofborehole water?(The atomic masses are Ca: 40.08; F: 19.00; O: 16; H: 1)
- The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of solubility and Ksp of calcium hydroxide: Trial 2: Final Buret reading (ml)-26.10; Initial Buret reading (ml)- 19.80; Temperature (Celcius)- 25 Voume of HCl used: Trial 2- 6.30mL 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Construct an ICE table for the reaction.3. Calculate the molar solubility (in mol/L) of OH- and Ca2+.4. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 5. Calculate the Ksp of Ca(OH)26. Compute for the percent error of the experimental value for Ksp of Ca(OH)2 with the literature…A 1.0 g sample containing urea was dissolved in water and diluted in a 100.00 mL volumetric flask. 20.00 mL aliquot was mixed with 30.00 mL water and subjected to digestion with concentrated H2SO4. The ammonia produced is collected in 30.00 mL of 0.0500 M HCl and the excess acid is back titrated with 0.0500 M NaOH, requiring 6.80 mL. Calculate the weight percent urea [(NH2)2CO, FW=60.06 g/mol] in the sample. Please use the factor label method in answering.A 1.0 g sample containing urea was dissolved in water and diluted in a 100.00 mL volumetric flask. 20.00 mL aliquot was mixed with 30.00 mL water and subjected to digestion with concentrated H2SO4. The ammonia produced is collected in 30.00 mL of 0.0500 M HCl and the excess acid is back titrated with 0.0500 M NaOH, requiring 6.80 mL. Calculate the weight percent urea [(NH2)2CO, FW=60.06 g/mol] in the sample.
- Following the monograph procedure, determine the weight in grams of sodium carbonate (MW-106 g/mol) used to standardize a 0.987 N sulfuric acid solution. 1. What specific type of titration is involved? A. Direct Acidemetry B. Direct Alkalimetry C. Residual Acidemetry D. Residual Alkalimetry 2. What is the analyte- titrant chemical reaction involved? A. Strong Base+Weak Acid B. Weak Acid+Strong Base C. Strong Acid+Weak Base D. Weak Base+Strong Acid 3. What is the preferred indicator for the chosen type of reaction above? A. Methyl Orange B. Penolphtalein C. Methyl Red 4. Consider that the burette was completely filled to the 0mp mark before titrating. What is the volume of titrant consumed based from the image below? A. 22.9 mL B. 22.2 mL C. 21.3 mL D. 22.7 mL 5. What is the unknown weight (grams) the problem? Your Answer:A 0.3045 g of CaCO3 primary standard was dissolved using concentrated HCl, evaporated to incipient dryness and quantitatively transferred to a 250 mL volumetric flask, and diluted to mark. A 10 mL of aliquot was then transferred to an Erlenmeyer flask, together with 5mL buffer and 5 drops of EBT indicator, and was used to standardize the EDTA titrant. The solution turned blue after the addition of 24.10 mL of EDTA. A blank correction was performed and was determined to be 0.4 mL. What is the concentration of EDTA obtained (MW CaCO3 = 100.0869 g/mol)?A 50.0 mL of 3.1% (w/v, g/mL) NaOH solution is mixed with 40.00 mL of 1.2% (w/v, g/mL) Na2CO3 solution. What volume of 0.087 M HCl will be required to titrate the resultant solution to bromocresol green indicator end point (Bcg pH transition range 3.8-5.4, Fwt of NaOH=40 g/mol, Na2CO3= 105.99 g/mol).