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Fractioned Distillation Microscale
Looking at this set up, are there any potential problems with it? Please explain.
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- Referring to the Al-Si Eutectic diagram discussed on the Phase Diagrams-Lever Rule handout, calculate the mass fraction of the phase, silicon, given a sample with 51.7 wt% aluminum at 576.99 ˚C.DATA Note: Use the videos as references except when data is provided here. Table 1. Selection of Recrystallizing Solvent. Solvents Dissolution at room temperature? (+ or −) Dissolution at elevated temperature? (+ or −) Distilled water - - Acetone + n/a 95% ethanol - + Toluene + n/a Solid sample: Naphthalene Table 2. Mass Measurements. Mass, g Sample solid 0.5021 Empty watch glass 35.7602 Watch glass with recrystallized sample 36.2485 Table 3. Melting Point Determination. Temperature, oC Appearance of Sample in Capillary Tube … Solid 78.4 Solid 79.3 Solid with signs of liquid 79.9 Solid, liquid 80.6 Liquid, solid 81.3 Liquid with signs of solid … Liquid Theoretical Melting Point, oC: 80.2°C (176.4°F) QUESTIONS Which solvent should be used as the recrystallizing solvent? Check if your chosen solvent satisfies all characteristics of a good…After a recrystallization, a pure substance will ideally appear as a network of Choose...smalllargeround Choose...clumpspowderscrystals . If this is not the case, it may be worthwhile to reheat the flask and allow the contents to cool more Choose...completelyquicklyslowly .
- solve as neatly as possible and show completesolution. Round your final answer to 4 decimal places and box / highlight all final answers. and all values must include proper units with proper conversion if needed in your solution. kindly folllow the format Given,Required,Solution subject physical chemistry 1. Calculate the mass of water vapor present in a room of volume 400 m3 thatcontains air at 290C when the relative humidity is 53.0%. Compute for the vaporpressure of water?Taylor was harvesting her beautiful, pure crystals via vacuum filtration from a methanol/water mixedsolvent system. She poured the solution containing her crystals into the Büchner funnel. Then sherinsed her flask with some warm methanol and poured that over the crystals resting in the Büchner…oops! Tell what happened and whydont provide handwritiing soution ...
- Matt was heating his methanol solvent in an E. flask on a hot plate to use for recrystallization. The TAcame by and noticed he didn’t have a stir stick or boiling chip in the flask and told him to use one,please. Matt dropped a stick in the flask and suddenly the liquid exploded out of the flask. Oops! Tellme why that happened. What should he have done instead?I s it possible to carry out steam distillation at a temperature higher than 100C at 1 atm? ExplainPolyethylene terephthalate is an example of synthetic material in Materials and Engineering. 1. Describe the relation of its building blocks in connection to its “bulk” (materials) properties. (No need for essay, just a brief scientific explaination!) If you may, please send link as well of the reference that you use for the answer).