Please choose an appropriate technique(s) to separate following compounds (it can be one, more than one, on none): Compound Melting Point Density Boiling Point Molar mass Phenol 40.5°C 1.07 g/cm 181.7°C 94.113 g/mol Toluene -95 °C 0.87 g/mL 111 °C 92.141 g/mol Simple Filtration Column Chromatography Distilation Crystallization/Re-Crystallization Separatory funnel None 1會云

Please choose an appropriate technique(s) to separate following compounds (it can be one, more than one, on none): Compound Melting Point Density Boiling Point Molar mass Phenol 40.5°C 1.07 g/cm 181.7°C 94.113 g/mol Toluene -95 °C 0.87 g/mL 111 °C 92.141 g/mol Simple Filtration Column Chromatography Distilation Crystallization/Re-Crystallization Separatory funnel None 1會云

Fundamentals Of Analytical Chemistry

9th Edition

ISBN:9781285640686

Author:Skoog

Publisher:Skoog

Chapter34: Miscellaneous Separation Methods

Section: Chapter Questions

Problem 34.2QAP

See similar textbooks

Similar questions

Which of the following characteristics of a reversed – phase chromatography? I. The stationary phase is polar II. The mobile phase is more polar than the stationary phase III. A less polar mobile phase has a lower eluent strength IV. A more polar mobile phase has a higher eluent strength V. The stationary phase is nonpolar a) I & III b) I & IV c) II & IV d) II & V e) II only
Anion and cation chromatography can be achieved by modifying? A. Type of dye B. Mobile phase C. Wavelength D. Stationary phase
1a) Hexane, CH3(CH2)4CH3, is found to have a long retention time when separated from a mixture. A column with a C18 (18-carbon chain) stationary phase and a methanol-water modal phase is used for the separation. Explain why hexane has a long retention time. 1b)You wish to chromatographically seperate a mixtureof the follwing compunds. Which of the two compounds will be most difficult to seperatate from one another? Why?
A mixture of three components is separated using paper chromatography, and each component is analyzed using absorption. With standards containing 100 ppm of each component run simultaneously, the following data were obtained: cmpd A, 0.72 absorbance; B, 0.55; C, 0.80. For the unknown mixture, the data obtined when run under identical conditions were as follows: cmpd A, 0.15 absorbance, B, 0.84; C, 0.75. a) Calculate the relative percentage composition of the unknown mixture. b) The distances traveled by the three components were 8.5, 6.3, and 5.5 cm, respectively. Sketch the appearance of the paper chromatogram. Label each spot. c) Calculate the Rf values if the solvent front is 18 cm.
Peak area is used for quantitative analysis in gas-liquid chromatography. True False
Which technique is based on the stronger attractionsome components have for the stationary phasecompared to the mobile phase? A. filtration D. chromatographyB. distillation E. sublimationC. crystallization
the efficiency of a chromatographic column improves the measure thata.increases the height of the theoretical dishesb.decreases the number of theoretical platesc.platform height is reducedd.None of the above Please explain it Provide clear handwriting and clear image
1. For the following chromatography state what the mobile phase is, stationary phase is, and what would elute first for each of the chromatography type... HPLC Gas Chromatography Ion Exchange Chromatography Size Exclusion Chromatography (SEC) Affinity Chromatography Reverse Phase Chromatography Normal Phase Chromatography
Which technique is more best from flirtation and centrifugation and how??
A student performs a separation by TLC on a silica gel platee that results in three spots. A red spot is measured 23 mm away from the original sample spot, a blue spot is 42 mm away, and a yellow spot is 49 mm away. the distance from the original spot to where the solvent stopped is 55 mm. a) calculate the Rf value for each componenet in the mixture (show work and report th correct number of significant figures) b) the silica gel plate is polar. rank the three componenets in the mixture from lowest to highest polarity. Explain your answer.
Waht is the composition of the reverse phase chromatography? non-polar stationary phase - non polar mobile phase polar stationary phase - non polar mobile phase polar stationary phase - polar mobile phase non- polar stationary phase - polar mobile phase
Please answer Questions 5-3, 5-4, and 5-5 (GC Gas Chromatography) 5-2. A sample mixture of ethyl benzoate (bp 212 Celsius) and dodecane (bp 216.2 Celsius) is injected on two GC columns.Column A has DC710 silicone oil as the stationary phase, and column B uses polyethylene glycol as the stationaryphase. Which substance would be certain to elute first from column A and would the same material be expected toelute first from column B? Which column, A or B, would be expected to give the better separation of these two substances? 5-3. Question 5-2 refers to separating a mixture of two high boiling liquids by gas chromatography. These materials havesimilar boiling points. List several GC variables and conditions that would make it easier to separate thesesubstances by gas chromatography. 5-4. Capillary GC columns have better resolution than packed columns even though the enormous surface area provided by the packing material is absent in capillary columns. Why? 5-5. Preparative GC requires…