IR Analysis – be sure to staple IR spectra to your report and fill in the following information. (Note there is a table in the attached image listing where the relevant peaks are. The product has an alkyl chain and an ester so look under the aliphatic hydrocarbons (means alkyl group) and ester categories in the table.a) Peak tablePeak Position cm-1Bond TypeFunctional Group b) Briefly explain based on you IR spectra how well your reaction worked. -(CH2)n- rock when n< 4-(CH2)n- rock when n>41370 and 1385 for (CH3)2CH-686d C-H (sym); doublet betweenUNIT 31INFRARED SPECTROSCOPYстTable 31.2 IR Characteristic Frequencies (±15 cm-1)Aliphatic hydrocarbons-CH32960st C-H2870st C-HR-OHan1460d C-H (asym)R-OH ar1380R-CH,–RCH-Cst C-Hst C-H-CH2-29252850RC-OKd C-HAr-OH1470720-725Ethers740-770R-O-AlkenesAmin=CH2st C-H (asym)st C-H (sym)st C-Hst C=C3085rut 2980R-NF=CH-3025C=C1640-1680R-CH=CH2RNF900-915985-1000R2C=CH2RHC=CHR (trans)RHC=CHR (cis)R2C=CHR880-900960-990d C-H out of planeAm665-730R-800-850AromaticsR3=CH-K.3020-3080st C-H; several bandsst C-C; phenyl ring skeletal;1580-1630R.1470-1530mono-substitutedoften doublets690-705 (s)730-775 (s)730-770 (s)680-725 (m)750-810 (s)860-900 (m)790-860 (s)3113 Dethe1,2-disubstituted1,3-disubstituted1,4-disubstituted1,2,4-trisubstitutedd C-H out of plane800-8601,2,3-trisubstituted860-900685-7201,3,5-trisubstituted770-810675-730800-8501,2,3,4-tetrasubst.1850-9001,2,4,5-tetrasubst. &790-8601,2,3,5-tetrasubst. &pentasubstituted850-900Alkynes=C-H-C=C- (terminal)-C=C- (central)3250-33502100-2150st C-HNitriles2180-2260st C=C-C=Nst C=C2220-2260st C=N(continued)Alcohols 90-Thu Oct 14 10:15:08 2021 (GMT-04:00)80-70-60-50-40-302010-0--10--20-4000350030002500200015001000500Wavenumbers (cm-1)Thu Oct 14 10:23:42 2021 (GMT-04:00)FIND PEAKS:Spectrum:Region:Absolute threshold: 35.088Sensitivity:Peak list:Thu Oct 14 10:15:08 2021 (GMT-04:00)4000.00400.0050Position:Position:Position:Position:Position:Position:416.28436.021242.201742.662932.722957.85Intensity:Intensity:Intensity:Intensity:Intensity:Intensity:-6.784-1.20010.0636.16327.41628.539mp2%Transmittance1742.661242.20

Given that the product has an alkyl chain and an ester group, the IR spectra is to be interpreted.

IR Analysis – be sure to staple IR spectra to your report and fill in the following information. (Note there is a table in the attached image listing where the relevant peaks are. The product has an alkyl chain and an ester so look under the aliphatic hydrocarbons (means alkyl group) and ester categories in the table. a) Peak table Peak Position cm-1 Bond Type Functional Group

IR Analysis – be sure to staple IR spectra to your report and fill in the following information. (Note there is a table in the attached image listing where the relevant peaks are. The product has an alkyl chain and an ester so look under the aliphatic hydrocarbons (means alkyl group) and ester categories in the table. a) Peak table Peak Position cm-1 Bond Type Functional Group

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter20: Molecular Mass Spectrometry

Section: Chapter Questions

Problem 20.11QAP

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