Mass spectral measurements were made on 10 replicate low concentration Pb-EDTA samples: 152.7, 114.6, 128.1, 143.1, 112.1, 181.5, 133.1, 137.7, 127.1, and 144.7 counts. Ten measurements of a blank had a mean measurement of 27.7 counts. A sample containing 2.00 µM Pb-EDTA gave a measurement of 1601 counts. Estimate the signal and concentration detection limits for Pb-EDTA. signal detection limit: counts concentration detection limit: µM

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter1: Introduction
Section: Chapter Questions
Problem 1.9QAP
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Mass spectral measurements were made on 10 replicate low concentration Pb-EDTA samples: 152.7, 114.6, 128.1, 143.1,
112.1, 181.5, 133.1, 137.7, 127.1, and 144.7 counts. Ten measurements of a blank had a mean measurement of 27.7 counts. A
sample containing 2.00 µM Pb-EDTA gave a measurement of 1601 counts. Estimate the signal and concentration detection
limits for Pb-EDTA.
signal detection limit:
counts
concentration detection limit:
µM
Transcribed Image Text:Mass spectral measurements were made on 10 replicate low concentration Pb-EDTA samples: 152.7, 114.6, 128.1, 143.1, 112.1, 181.5, 133.1, 137.7, 127.1, and 144.7 counts. Ten measurements of a blank had a mean measurement of 27.7 counts. A sample containing 2.00 µM Pb-EDTA gave a measurement of 1601 counts. Estimate the signal and concentration detection limits for Pb-EDTA. signal detection limit: counts concentration detection limit: µM
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