Lithium in a sample is determined by flame emission spectrometry, using a standard additionscalibration. 100µL of sample diluted to ImL gives an emission signal of 6.7 units. A similarsolution to which 10 uL of a 0.010M solution of LINO; added gives a signal of 14.6 units.Assuming linearity between the emission signal and the lithium concentration, what is theconcentration of lithium in the sample in ppm?5.91.72.11.14.6

If 10 microlitres of 0.010M of lithium nitrate on addition gives 14.6 units, then the sample without…

Answered: Lithium in a sample is determined by…

Principles of Instrumental Analysis

7th Edition

ISBN:9781305577213

Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch

Chapter1: Introduction

Section: Chapter Questions

Problem 1.9QAP

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Inductively coupled plasma–optical emission spectrometry (ICP-OES) was used for the determination of cadmium using indium as an internal standard. A solution containing 2.15 ppm Cd2+ and 5.76 ppm In3+ gave signals of 19,291 and 37,190 counts for cadmium and indium, respectively. A 0.01652 g sample was dissolved in acid and quantitatively transferred to a 250.0 mL volumetric flask. A 1.00 mL aliquot of 264.5 ppm In3+ was added and the flask was diluted to volume with deionized water. ICP-OES analysis of the sample solution gave signals of 31,109 and 118,941 counts for cadmium and indium, respectively. What was concentration of the Cd2+ in the sample? Give answer all questions with explanation
UV-Visible spectroscopy is used to determine the content of an analyte in a capsule. Weigh 100.0 mg of the capsule contents (total weight of contents 500 mg), add 2.0 mL of 0.05 M NaOH, filter the flask, and make up to 25.00 mL with NaOH. The measured transmittance of this solution is 33.0%. The analyte standard is prepared by dissolving 10.0 mg of standard in 25.00 mL of 0.05 M NaOH, then taking 10.00 mL of that solution and diluting to a final volume of 50.00 mL where the transmittance is obtained from 44.0%. Calculate the content of the analyte in the capsule.
For the determination of Fe3 +, 25 mL of sample taken from sea water is diluted to 100 mL and a quantity of the obtained solution is taken and Fe3 + is determined by atomic absorption spectrophotometer. The absorbance values of the standard and sample solutions are below, and calculate the Fe3 + concentration in sea water in mg / L by drawing the relevant graph.Solution Absorbance1 mg / L Fe3 + 0.04095 mg / L Fe3 + 0.205110 mg / L Fe3 + 0.411615 mg / L Fe3 + 0.620820 mg / L Fe3 + 0.8222Sample Solution 0.5155

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