Simple Distillation The temperature was 76o C when the first drop of distillate was collected. Liquid was collected and the temperature gradually rose to 124 o C. Fraction 2 was taken when liquid was distilling at 124o C. Fractional Distillation The temperature was 77o C when the first drop of distillate was collected. Liquid was collected until the temperature reached 78 o C, then the temperature dropped. The temperature of the hot plate was increased and a second fraction of liquid was collected at 126 o C. a.) Based on the boiling points observed when the fractions were collected, what is the identity of the unknown compound isolated in fraction 1 and Fraction 2?

Chemistry & Chemical Reactivity
10th Edition
ISBN:9781337399074
Author:John C. Kotz, Paul M. Treichel, John Townsend, David Treichel
Publisher:John C. Kotz, Paul M. Treichel, John Townsend, David Treichel
Chapter13: Solutions And Their Behavior
Section13.5: Colloids
Problem 1.1ACP: The blue line on the diagram illustrates the effect of using fractional distillation to separate a...
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Simple Distillation

The temperature was 76o C when the first drop of distillate was collected.

Liquid was collected and the temperature gradually rose to 124 o C.

Fraction 2 was taken when liquid was distilling at 124o C.

Fractional Distillation

The temperature was 77o C when the first drop of distillate was collected.

Liquid was collected until the temperature reached 78 o C, then the temperature dropped.

The temperature of the hot plate was increased and a second fraction of liquid was collected at 126 o C.

a.) Based on the boiling points observed when the fractions were collected, what is the identity of the unknown compound isolated in fraction 1 and Fraction 2?

 

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