101 Ex4 ReportTemplate_2309

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University of Victoria *

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101

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Chemistry

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Feb 20, 2024

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docx

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Uploaded by LieutenantDeer3412

1 Report for Chem 101 Laboratory Exercise #4 Spectrophotometric Determination of Salicylic acid 1 Using Microsoft Word, students are to insert responses in all yellow highlighted areas. It is recommended that the report be completed without changing font size, column width, row width, margins, and highlights. The completed report must be uploaded to the CHEM 101 Brightspace site as a .pdf file by the due date posted on Brightspace. All answers must be the student’s own work without assistance from others. Only reports which are completed using the template will be marked. Name: Lab Section: Quad: Date: Abstract The % mass of salicylic acid in an acne cleanser produced by Johnson & Johnson, was determined to be 0.054% by measurement of the absorbance that was determined from a calibration curve. This was found to be 3.8% of the advertised value. Data/Results Table 1. Experimentally measured absorbances (A) and calculated concentrations (conc) for the standard salicylic acid solutions. The observed data inserted in this table must be consistent with the observed data written in your laboratory notebook with the correct units. conc Stock salicylic solution 0.002917M A conc standard solution #1 0.244 0.00011668M = 1.17x10^(-4)M (with sig figs) standard solution #2 0.831 0.0005834M = 5.83x10^(-4)M (with sig figs) standard solution #3 1.390 0.0011668M = 1.167x10^(-3)M (with sig figs) Table 2. Determination of the amount of salicylic acid in the acne cleanser. The observed data inserted in this table must be consistent with the observed data written in your laboratory notebook with the correct units. Volume of acne cleanser used in the analysis 0.3mL Acne cleanser aliquot #1 Acne cleanser aliquot #2 Acne cleanser aliquot #3 Absorbance 1.196 1.207 1.189 [salicylic acid] from curve 0.0009668M 0.0009772M 0.0009608M Moles of salicylic acid 2.4 x10^(-5) moles 2.4 x10^(-5) moles 2.4 x10^(-5) moles
2 in 25.00 mL Mass of salicylic acid in 25.00 mL 0.0033g 0.0045g 0.0033g Mass of salicylic acid in 1.00 mL of acne cleanser 0.00013g 0.00018g 0.00013g %mass of salicylic acid in acne cleanser 0.048% 0.066% 0.048% % comparison to advertised value 3.8% Calibration curve for standard solution of salicylic acid (cut and paste from Excel) and determination of the salicylic acid concentration in an acne cleanser by interpolation 0 0 0 0 0.2 0.4 0.6 0.8 1 1.2 1.4 1.6 f(x) = 1085.85 x + 0.15 R² = 0.99 Spectrophotmetric determination of salicylic acid at 535nm Concentration of Salicylic Acid Absorbance at 535nm _ Algebraic Equations (see page 12 of the Chem 101 lab manual) Concentration of a standard solution = (moles of standard solution)/(volume of solution)
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