Project 3: Oxidation-Reduction

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Santa Clara University *

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800

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Chemistry

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Oct 30, 2023

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pdf

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5

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Genem| Reaction Preparhon of NaOCI ol Na Reaction Z Na0Gl, CHy CO H _ Acetone, A A 50°C t+ MNaOH —> NalCl + 06l + COH600H ——> HOCI Mechanism : Oxidqtion 0 NaCl + CHy 000~ Na"
Extraotion Flowchart : 0Oxidgtion 300 mg of ‘l'-'f@r'l'-bu'lyloflolohexanal w/ 4 mk of acetone + 0.50 mk glacial acetic acid + #0 mk of NqOCI o O i § it T added 10 m}- w/ 5Sm- of & sodium bicarbongte Repeat ex-I:Fwo-hon then 5mk of DI H0 w/ 10 mk hexdanes n Remove I stopper £ \[\? qufioq_ o & ~— Drqin agqueous A % Dmin hexanes (‘# I:nor 1::\‘!0 a beaker | d d w?“?nh;rglmu 3 sodium” sultate Extraction Flowchart : Redveton w/ MPY |00 mg of +-1'ezrl-—bu13IoUolohexanane w/ 0-4mk of acetne, 4 mk of isopropyl alcohdl, 10g of alumnium isopropoxide L T N\ ”fl.fiflfi% % 20 mk H,0 Wash fwice w/ added 10 mk of ether Wash ether w/ 10 ml DI HLO twice .. Mq$0 & S~ D 80us A —L % Drgin ether % rIqalmer“’::\-lu layer and d a beaker A w/ qnhjolrous A
General Reachon : Reduction 0 0H H Al (0iPr), I 7 I H t OH iPrOH Reaction Mechanism : MPV Reducthon 0 H A\ [1] :0H /l\"\m/"/k\/)\ /k"\ -0 e— | /M\..+ 10 /0
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