Zimmerly

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School

Ohio State University *

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Course

2540

Subject

Chemistry

Date

Dec 6, 2023

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pdf

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8

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Chem 2540 Callam/Paul – AU23 Four for you Glen Coco! You go, Glen Coco! AU22 D ISTILLATION AND G AS C HROMATOGRAPHY R EPORT PREPARED BY : D ATE : L AB ROOM : TA: I NSTRUCTIONS : 1. Begin by obtaining the “Distillation Data Set” from Carmen. 2. Simple Distillation a. Using the provided rulers, calculate the t R in seconds and area under the peak in squared millimeters for each major peak present. Show your work. b. Using your knowledge of gas chromatography, identify which peak corresponds to which compound: 1-propanol and THF. 3. Fractional Distillation a. Using the provided rulers, calculate the t R in seconds and area under the peak in squared millimeters for each major peak present. Show your work. b. Calculate the t R value in seconds for each peak on the 4-part reference chart. c. Compare the peak t R values on for the distillate and pot fractions to the reference t R values you just calculated. d. Using your knowledge of gas chromatography, identify which peak corresponds to which compound: ethyl acetate, methylcyclohexane, pentane, toluene. 4. Submit your completed worksheet and the “Distillation Data Set” as a single file to Carmen. ethylacerate 77C D 1012 it 36 C toulene 110.69 Madison Zimmerly 10/22/2023 Zoie Pettito 460
Distillation and Gas Chromatography Digital Lab Report Chem 2540 Four for you Glen Coco! You go, Glen Coco! AU22 S IMPLE D ISTILLATION Distillate Injection Pot Injection Component 1 identity: _________________ Component 2 identity: _________________ Space for calculations: Peak 1 Peak 2 t R (s) Area (mm 2 ) Percent Composition Peak 1 Peak 2 t R (s) Area (mm 2 ) Percent Composition iii s g 13.867 4 125 it 6 15 93.85 THE 1 propanol j 41 26.5 114.5mm Wiz W 83.75mm 96mm 50mm 6mm tmin 1.0661min Emin 6 114.5 0687mm 63.960 Aca h 141 124 17 Wya w 132.5 94 87.5 6.5 2 D9 gg 1.81ynin 6fmm 6.5.17 110.5mm 108.840 HA 110.5 687 797.50 in tri ii tn A N Yew total area A tAz Y g 86.14 0 percent composition e 100 i It 10.5 tr 551 064 65.40 totalt 768.25 91 6014 4 103 0721 42 853 9 97.560 12 93.85 0
Distillation and Gas Chromatography Digital Lab Report Chem 2540 Four for you Glen Coco! You go, Glen Coco! AU22 F RACTIONAL D ISTILLATION Distillate Injection Pot Injection Reference Component 1 identity: _________________ Component 2 identity: _________________ Space for calculations: Peak 1 Peak 2 t R (s) Area (mm 2 ) Percent Composition Peak 1 Peak 2 t R (s) Area (mm 2 ) Percent Composition Peak 1 Peak 2 Peak 3 Peak 4 t R (s) al D 15.6 154 28.2 16 Tf 60 15.6 90.59010 9.417 2 21 60 28.8 28.2 3 659.60 82.8 3124285 88 26 824 73.189 ry 12 160 150 15.6 28.8 82.8 150 trisarti Emin A N Yew total area A tAz I a hazan Pt percent composition e.no tri again Peak 8.51 ftp.zsmm YzW 1.5mm.Peak2 k8tr tgym 6o tri 2 FI gtrz 23qglEn h8 DywezAi peaky nano 96 44 Ai Mala 170 42W 2mm total area 120.25 i Tons oo 7s 35525 26.82 0
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