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Course
2540
Subject
Chemistry
Date
Dec 6, 2023
Type
Pages
8
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Chem 2540
Callam/Paul – AU23
Four for you Glen Coco! You go, Glen Coco!
AU22
D
ISTILLATION AND
G
AS
C
HROMATOGRAPHY
R
EPORT PREPARED BY
:
D
ATE
:
L
AB ROOM
:
TA:
I
NSTRUCTIONS
:
1.
Begin by obtaining the “Distillation Data Set” from Carmen.
2.
Simple Distillation
a.
Using the provided rulers, calculate the t
R
in seconds and area under the peak in squared
millimeters for each major peak present. Show your work.
b.
Using your knowledge of gas chromatography, identify which peak corresponds to which
compound: 1-propanol and THF.
3.
Fractional Distillation
a.
Using the provided rulers, calculate the t
R
in seconds and area under the peak in squared
millimeters for each major peak present. Show your work.
b.
Calculate the t
R
value in seconds for each peak on the 4-part reference chart.
c.
Compare the peak t
R
values on for the distillate and pot fractions to the reference t
R
values you just
calculated.
d.
Using your knowledge of gas chromatography, identify which peak corresponds to which
compound: ethyl acetate, methylcyclohexane, pentane, toluene.
4.
Submit your completed worksheet and the “Distillation Data Set” as a single file to Carmen.
ethylacerate
77C
D
1012
it
36
C
toulene
110.69
Madison Zimmerly
10/22/2023
Zoie Pettito
460
Distillation and Gas Chromatography Digital Lab Report
Chem 2540
Four for you Glen Coco! You go, Glen Coco!
AU22
S
IMPLE
D
ISTILLATION
Distillate Injection
Pot Injection
Component 1 identity: _________________
Component 2 identity: _________________
Space for calculations:
Peak 1
Peak 2
t
R
(s)
Area (mm
2
)
Percent Composition
Peak 1
Peak 2
t
R
(s)
Area (mm
2
)
Percent Composition
iii
s
g
13.867
4
125
it
6
15
93.85
THE
1
propanol
j
41
26.5
114.5mm
Wiz
W
83.75mm
96mm
50mm
6mm
tmin
1.0661min
Emin
6
114.5
0687mm
63.960
Aca
h
141
124
17
Wya
w
132.5
94
87.5 6.5
2
D9
gg
1.81ynin
6fmm
6.5.17
110.5mm
108.840
HA
110.5
687
797.50
in
tri
ii
tn
A
N
Yew
total
area
A
tAz
Y
g
86.14
0
percent
composition
e
100
i
It
10.5
tr
551
064
65.40
totalt
768.25
91
6014
4
103
0721
42
853
9
97.560
12
93.85
0
Distillation and Gas Chromatography Digital Lab Report
Chem 2540
Four for you Glen Coco! You go, Glen Coco!
AU22
F
RACTIONAL
D
ISTILLATION
Distillate Injection
Pot Injection
Reference
Component 1 identity: _________________
Component 2 identity: _________________
Space for calculations:
Peak 1
Peak 2
t
R
(s)
Area (mm
2
)
Percent Composition
Peak 1
Peak 2
t
R
(s)
Area (mm
2
)
Percent Composition
Peak 1
Peak 2
Peak 3
Peak 4
t
R
(s)
al
D
15.6
154
28.2
16
Tf
60
15.6
90.59010
9.417
2
21
60
28.8
28.2
3
659.60
82.8
3124285
88
26
824
73.189
ry
12
160
150
15.6
28.8
82.8
150
trisarti
Emin
A
N
Yew
total
area
A
tAz
I
a
hazan
Pt
percent
composition
e.no
tri
again
Peak
8.51
ftp.zsmm
YzW
1.5mm.Peak2
k8tr
tgym
6o
tri
2
FI
gtrz
23qglEn
h8
DywezAi
peaky
nano
96
44
Ai
Mala
170
42W
2mm
total
area
120.25
i
Tons
oo
7s
35525
26.82
0
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Please written by hand
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ABookmark
Gonzalez, Marianna
RETAKE S2 Chem Unit 9 Common Unit Assessment / 5 of 10
II Pause
O Help -
Use the information to answer the following question.
Ammonia (NH3) readily dissolves in water to yield a basic solution.
NH3 + H20 NH4+ + OH
How is this substance classified?
O A. Arrhenius Base
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Com X
Bb Mas X
Mas X
Hom X
K! Kahx
Exan X
K! Kah X
Mitc X
КI Kah X
K Kah x
K! Kah x
Kah x K Kahx
C
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b. 1
(a).
;Give the correct interpretation of the interval in part
c. Extra Credit: Does this interval support Don's claim? Why?
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n eFundi : NCHE 121 1-
NCHE 121 - Test 8 - Ve X
G c8h12i iupac name - C X
b My Questions | bartleb x
R° (PDF) The Fourth Indu: X
R° (PDF) In dis tree - 4 W x
A docs.google.com/forms/d/e/1FAlpQLScN5aWTObzfQAgIF5ETgigA7N4LhreJo3ILGJ6Zwl0D7iboNQ/formResponse
Question 3: Which of the following intermolecular forces would you expect
between the haloalkane molecules in Figure 3? *
Hydrogen bonds
Dipole-dipole forces
Dipole-induced dipole forces
Induced dipole-induced dipole forces
Figure 3
17:30
P Type here to search
38°C Partly sunny
2021/11/04
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No written by hand solution
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In part A.3. as the sample cools, moisture from the atmosphere condenses on the outside of the
evaporating dish, before the mass is measured. The presence of the condensed moisture will
the reported TDS in the water sample.
O leave unchanged
decrease
double
O half
O increase
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h.
j.
k.
1.
m.
n.
0.
p.
H3C
Ph
CI
CH3
di
HO
H3C/11
Ph
MgCl
CH3
-CH3
H
Li
-MgBr
H
1) LiCuPh2
2) H30Ⓒ
Mg
THF
H₂O
1) NaBH4
2) H300
1) Å
2) H3O+
excess CrO3
aq. H₂SO4
acetone
1) LICU(CH3)2
2) H300
CrO 3
pyridine
1) CO₂
2) H30
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Need help
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119 X
My Course X
Macmillan: X
Course Mo X
What is the FORMULA for the limiting reagent?
Submit Answer
Sections 5 X
.com/static/nb/ui/evo/index.html?deploymentid=5735112480241329813180832311&elSBN=9781305862883&id=1707786042&snapshoti...
Use the References to access important valdes ir needed for this question.
900
For the following reaction, 9.43 grams of carbon (graphite) are allowed to react with 28.5 grams of oxygen gas.
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What is the maximum amount of carbon dioxide that can be formed?
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HOMEWOR X
MacBook Air
MindTap - C X GI
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4. Price the Prescription using the Professional Fee method.
Rx
Potassium chloride
40 mEq
NaCl
30 mEq
M. In pp. Tab. No. 20
Sig Dissolve the contents of 1 paper tab in 1 glass of water, taken after breakf
- P35.00
Given: Professional Fee
each mEq KCI
=0.075 g
%3D
each mEq NaCi
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%3D
Cost of 100 g KCI
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%3D
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CHEM 1221 GRADED TEST 4
x +
UPLOAD YOUR HANDWRITTEN AND COLLATED PDF FILE HERE. *
General Instructions
>
Show the complete and organize sokition, Write your onswer wilth four decimal places and enclose them in
a box Solve n neally as possible. Messy work wil be given necessory deductons.
Toke a clear photo of your handwritten work and UPLOAD I os a COLLATED pdf at google fom using the
file le fomat
SURNAMEGIVENNAMEINITALS CLASSCODE GI PROB
EXAMPLE DELACRUZI 1234 GII PROBI
PROBLEM 3:
A chloride ion is added in a solution containing 4.144g/L of Pb**
and 1.088g/L Ag*. Determine the chloride ion concentration to
begin precipitation of the salt formed and which will
precipitate first.
1 Add file
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9 CHEM 1221 GRA.
*Untitled - Note.
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ASSAY
Calibration solutions
Calibration solutions of naproxen in the range 5 – 25 μg/mL were prepared.
Sample preparation
20 tablets weighing 12.3819 g were crushed to a fine powder. A portion of the powder (145.4 mg) was shaken with approximately 150 mL of acetic acid (0.05 M) for 5 min and then made up to volume in a 250 mL volumetric flask (stock solution). Approximately 50 mL of the stock solution was filtered and a 25 mL aliquot was diluted to 100 mL in a volumetric flask. 10 mL of the resulting solution was further diluted to 100 mL with acetic acid (0.05 M).
Analysis
The standards and sample solutions were analyzed by HPLC under the following conditions:
Column: octadecylsilyl (ODS), 4.6 mmx150 mm,
mobile phase: acetonitrile : 0.05 M acetic acid (85:15),
flow rate: 1 ml/min,
UV detection at 243 nm.
Results:
A calibration curve of concentration versus peak area was constructed for the standard solutions and gave the straight-line equation: y = 3555.6x + 85, r = 0.9999
The area…
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%V. II. ¹8
ش1 (442 CHEM) كيمياء فيزيائية (3)
Question 2
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Marked out of 2.00
Dashboard My courses / CHEM 442 1 / Topic 2
/ Quiz 4
m₂=9.1x10-³1 Kg
h=6.626x10-34 J.S
elearning.yu.edu.jo/sur
a. 6.4e-17 J
O b. 1.6e-16 J
c. 9.5e-17 J
d. 1.3e-16 J
O e. 1.9e-16 J
Calculate the lowest possible energy for an electron
confined in a 1D-box of length equal to 17.8 pm.
Given:
=
|||
1:1
O
Time left 0:13:03
Next page
A
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Please see picture attached
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3.
+
3HCI
B
H.
H.
H.
と-
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UPVOTE WILL BE GIVEN! PLEASE WRITE THE SOLUTIONS LEGIBLY. THANK YOU! ANSWER IN 3 DECIMAL PLACES.
CHEMISTRY! NO LONG EXPLANATION NEEDED.
A 10 ml of concentrated acetic acid was added in a sufficient quantity of water to make 350 ml of the acid solution.
SG acetic acid = 1.05
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Select one:
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Ob. 55%
OC. 65%
O d. 35%
Snot too much of a compound on tha TIC nlato wIould make2
TOSHIBA
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A
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9.
T Y
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FIG ý Hi
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6
PLEASE PROVIDE THE INTERPRETATION OF ALL SAMPLES FOR HELPFUL RATINGS. THANK YOU.
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- Determine the percent completion for both you distillation and your collegues whose data you obtained. (What percentage (by weight) of the octane/isooctane mixture was collected in the distillate vial?arrow_forwarda. 27 centipoise (cP) to g.s1.cm1 b. 130 Btu-lb1 to kcal-g C. 997 kg m3 to lb-ft3 Notes: 1 m= 100 cm, 1 cP = 103 kg-m1-s1, 1 Btu = 0.252 kcal, 1 lb = 453.6 g, 1 kg = 1000 g, 1 m³ = 1000 L, 1 ft=0.3048 marrow_forwardPlease written by handarrow_forward
- 1:39 PM Fri Apr 30 100% AA A testnavclient.psonsvc.net G Cannot MY eCLASS .. B Homepage -. O Schoolnet TestNav Favorites Review ABookmark Gonzalez, Marianna RETAKE S2 Chem Unit 9 Common Unit Assessment / 5 of 10 II Pause O Help - Use the information to answer the following question. Ammonia (NH3) readily dissolves in water to yield a basic solution. NH3 + H20 NH4+ + OH How is this substance classified? O A. Arrhenius Base Exhibits B. Arrhenius Acid C. Bronsted-Lowry Acid D. Bronsted-Lowry Basearrow_forward20,18,2,4,15,15,10 Using these data, construct a 80% confidence interval for the average net change in a student's score after completing the course. Assume the population is approximately normal. Construct the 80% confidence interval. Round your answer to one decimal place.arrow_forwardCom X Bb Mas X Mas X Hom X K! Kahx Exan X K! Kah X Mitc X КI Kah X K Kah x K! Kah x Kah x K Kahx C session.masteringchemistry.com/myct/itemView?assignmentProblemID=134214560 Apps New Tab Effect of Salinity on... Sleep Disorders | M... P Philo American Journal ... Zeeshan JBAS Ic Wait for Next Quest... oramge juice Effect carrow_forward7. Don believes that fewer than one-third of the students at his college hold part-time jobs while in school. To investigate this, he randomly surveyed 116 students and found that 32 students held part-time jobs. a. ( - Provide a 90% confidence interval for the population proportion of students that hold a part-time job. b. 1 (a). ;Give the correct interpretation of the interval in part c. Extra Credit: Does this interval support Don's claim? Why?arrow_forwardn eFundi : NCHE 121 1- NCHE 121 - Test 8 - Ve X G c8h12i iupac name - C X b My Questions | bartleb x R° (PDF) The Fourth Indu: X R° (PDF) In dis tree - 4 W x A docs.google.com/forms/d/e/1FAlpQLScN5aWTObzfQAgIF5ETgigA7N4LhreJo3ILGJ6Zwl0D7iboNQ/formResponse Question 3: Which of the following intermolecular forces would you expect between the haloalkane molecules in Figure 3? * Hydrogen bonds Dipole-dipole forces Dipole-induced dipole forces Induced dipole-induced dipole forces Figure 3 17:30 P Type here to search 38°C Partly sunny 2021/11/04arrow_forwardNo written by hand solutionarrow_forwardIn part A.3. as the sample cools, moisture from the atmosphere condenses on the outside of the evaporating dish, before the mass is measured. The presence of the condensed moisture will the reported TDS in the water sample. O leave unchanged decrease double O half O increasearrow_forwardAaBbCcDd AaBbCcDd AaBbC AaBbCct AaB AaBbCcD 1 Normal 1 No Spac... Heading 1 Heading 2 Title Subtitle 1 Styles Name HHHHH ||||| H-C-C=C-C-C-H | H || HH Name H H-C-H C=C F -H —H H C 1 B. H H Name H H H H1C C H Η Η Η Η Η Η | | | | | | H-C₁-C₂-C₂-C-C-C-H II HH H H-C-H H -H y Find ✓ Replace Select Editing 14°C Cloudy A Dictate Voice F Fooarrow_forwardh. j. k. 1. m. n. 0. p. H3C Ph CI CH3 di HO H3C/11 Ph MgCl CH3 -CH3 H Li -MgBr H 1) LiCuPh2 2) H30Ⓒ Mg THF H₂O 1) NaBH4 2) H300 1) Å 2) H3O+ excess CrO3 aq. H₂SO4 acetone 1) LICU(CH3)2 2) H300 CrO 3 pyridine 1) CO₂ 2) H30arrow_forwardarrow_back_iosSEE MORE QUESTIONSarrow_forward_ios
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