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- Mr. Clean recently bought a laboratory-grade sodium carbonate from a chemical company known as Brand X. He was supposed to use it in the production of detergents. Unfortunately, he was scammed by the company. He suspected that he purchased a crude sodium carbonate so he tasked the Quality Assurance Department to determine the components of the purchased chemical. The chemist assigned to analyze the sample used double indicator method. For the standardization of HCl titrant, 0.1025 g Na2CO3 of 99.5% purity (FW: 106.00) required 8.20 mL of the titrant to reach the phenolphthalein endpoint. FW: NaOH (40.00), NaHCO3 (84.01), Na2CO3 (106.00) a. What is the molarity of the titrant? The chemist obtained a 3.150 g sample and dissolved it in distilled water to produce a 50.0 mL solution. An aliquot of 10.00 mL was obtained and diluted in a 100.0 mL volumetric flask. A 50.00-mL aliquot of the diluted sample was taken and it required 25.70 mL of titrant for the methyl orange endpoint, while…1. 1093-g sample of impure Na2CO3 was analyzed by residual precipitimetry. After adding 50.00 mL of 0.06911 M AgNO3, the sample was back-titrated with 0.05781 M KSCN, requiring 27.36 mL to reach the endpoint. The percentage Na2CO3 (MW = 106.0 g/mole) in the tested sample is ________ % ? Note: Express final answer using least number of significant figures. 2. The alkalinity of natural waters is usually controlled by OH- (MW = 17.01 g/mole), CO3-2 (MW = 60.01 g/mole), and HCO3- (MW = 61.01 g/mole), which may be present singularly or in combination. Titrating a 10.0-mL sample to a phenolphthalein endpoint requires 38.12 mL of a 0.5812 M solution of HCl, and an additional 18.67 mL of the same titrant to reach the methyl orange endpoint. The composition of the sample is _________% CO3-2 and ___________ % OH- Note: Express final answers using least number of significant figures.A piece of Gold weighing 12,359 Kg is suspected of being contaminated with Iron. To perform an instrumental analysis and To confirm whether or not it contains Fe, a portion of the sample (0.954 g) is taken from the piece and dissolved with 25 mL of aqua regia. Heats up For its complete dissolution, it is cooled and made up to 100 mL. A 10 mL aliquot is taken from this solution and made up to 50 mL. From This last solution is given the appropriate treatment to visualize Fe+2, for which the 1,10-phenanthroline reagent is added. (it forms a complex that is red in color) and is taken to a visible spectrophotometer and with a 12 mm cell a absorbance of 0.45. Previously, a calibration curve of Fe+2 was obtained under the same instrumental conditions obtaining the following data: (view table) Calculate the purity of the gold piece, assuming impurities only due to Fe.
- 1ml of 1mg/ml of diluted aspirin powder solution is titrated by 0.005M NaOH. Before titration, 5 ml ethanol, 14 ml CO2 free water, and 4 drops bromothymol blue indicator is added into diluted aspirin powder solution. Mass of 0.005M NaOH used is obtained by weight titration = 1.1384g . [Molar mass of aspirin =180.15]; for solution, 1g=1mL at 25 degree Celcius. Calculate the purity of the powder.In the standardi zation of HCl using pure anhydrou s sodium carbonate as primarystandard for methy l orange as indica tor , 1.0 mL HCl was found to be equiva lent to 0.05gof sodium carbonate (MW =106). The no rmality of HCl isThe SO2 present in air is mainly responsible for the phenomenon of acid rain. The concentration of SO2 can be determined by titrating against a standard permanganate solution as follows: 5SO2 + 2MnO4- + 2H2O ---> 5SO42- + 2Ms2 + 4H+ Calculate the number of grams of SO2 in a sample of air if 4.90mL of 0.00700M KMnO4 solution are required for the titration. Be sure your answer has the correct number of significant digits.
- Calcium fluoride is considered as a relatively insoluble compound and therefore lime or slakedlime has been considered as a possible material to remove excess fluoride in water of boreholesin certain parts of the country. The solubility product of CaF2 is Ksp = 3 x 10 – 11 and that ofCa(OH)2 isKsp =8x10-61. How much lime can be added to the water to remove 10 mg of F- ion per litre ofborehole water?(The atomic masses are Ca: 40.08; F: 19.00; O: 16; H: 1)A Medical Technology student was given a capsule of a multivitamins and she was asked to determine the % by mass (w/w) of ascorbic acid present in the capsule. The student analyzed the 2.001 g sample using volumetric titration. The following data was generated in the analysis: KIO3 + 5KI + 6H+ → 3I2 + 6K+ + 3H2O C6H8O6 + I2 → C6H6O6 + 2I- + 2H+ Table 1. Standardization of KIO3 Molarity of Ascorbic Acid Standard Solution 0.03542 M Volume of Ascorbic Acid 25.00 mL Volume of KIO3 8.70 mL Molarity of KIO3 ______________M Table 2. Determination of Ascorbic Acid Concnetration Initial burette reading, KIO3 0.00 mL Final burette reading, KIO3 33.60 mL Volume consumed, KIO3 33.60 mL MM of Ascorbic Acid 176.12 g/mole choices 7.30% 30.1% 33.6% 32.5%Aspirin powder = 0.8110g MW of Aspirin = 180g.mol-1 Volume of 0.5N HCl consumed in back titration = 23.50mL Volume of 0.5N HCl consumed in blank titration = 44.50mL Percent purity (USP/NF) = Aspirin tablets contain NLT 90.0% and NMT 110.0% of the labeled amount of aspirin (C9H8O4) What is the calculated weight (in grams) of pure aspirin?..
- A 0.1093-g sample of impure Na2CO3 was analyzed by the Volhard method. After adding 50.00 mL of 0.06911 M AgNO3, the sample was back-titrated with 0.05781 M KSCN, requiring 27.36 mL to reach the endpoint. Report the purity of the Na2CO3 sample. [Ans. 90.9 % (w /w )]0.9563 g KHCO3 (M.r.(KHCO3) = 100.12 g/mol (mg/mmol)) have measured, and 50.0 cm3 stock solution have been prepared from it. 10.00 cm3 individual samples from it was titrated with HCl titrant in order to determine its concentration. The average HCl consumption was 19.18 cm3. The same HCl solution with were used to determine the concentration of NaOH titrant. The base consumption for 20.00 cm3 HCl was 21.35 cm3 NaOH. 1. concentration of HCl 2. concentration of NaOHA saturated solution of magnesium hydroxide is prepared and the excess solid magneisum hydorixed is allowed to settle. A 25.0 mL aliquot of the saturated solution is withdrawn and transfered to a flask, two drops of inficator are added. A 0.00053 M HCL is dispensed from a buret into a solution. The solution changes color after the addition of 13.2 mL. What is the Ksp of magnesium hydroxide?