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- Patients undergoing an upper gastrointestinal tract laboratory test are typically given an X-ray contrast agent that aids with the radiologic imaging of the anatomy. One such contrast agent is sodium diatrizoate, a nonvolatile water-soluble compound. A 0.378-m solution is prepared by dissolving 38.4 g sodium diatrizoate (NaDTZ) in.l.60 102 mL water at 3 1.2C (the density of water at 31.2C is 0.995 g/cm3). What is the molar mass of sodium diatrizoate? What is the vapor pressure of this solution if the vapor pressure of pure water at 31.2C is 34.1 torr?A student was given a stock aluminum(III) solution with a concentration of 5.000 parts per million (ppm). (ppm are defined as mg/L for dilute aqueous solutions.) The student prepared five 100 mL standard solutions and an unknown as described in the procedure section of the experiment. The absorbance of each solution was read at 565 nm, using the blank to set zero absorbance. The results are tabulated below. Solution Volume of Al(III) stock solution used (mL) Absorbance 1 8.00 0.701 2 6.00 0.548 3 4.00 0.378 4 2.00 0.208 5 1.00 0.123 Unknown --- 0.534 3. What is your best estimate of the Al(III) concentration of the unknown sample in the cuvet based upon where its absorbance falls on the standard curve?Following the monograph procedure, a 724-mg of aspirin (MW-180 g/mol) dissolved in 18.5 ml of cold neutralized alcohol. This solution was then initially titrated with 0.101 N sodium hydroxide solution, then later neutralized with 0.104 N sulfuric acid. What is the percentage purity of sample?
- You determine the acetic acid (HOAc) content of vinegar by titrating with a sodium hydroxide standard solution to a phenolphthalein (an indicator) end point. An approximately 5-mL sample of vinegar is weighed on an analytical balance in a weighing boat and this is found to be 5.0268 g. The standard deviation in making a single weighing is 0.2 mg. The sodium hydroxide must be accurately standardised (this means its concentration must be accurately determined) by titrating known mass of high-purity potassium hydrogen phthalate, and three such titrations give molar concentrations of 0.1167, 0.1163 and 0.1164 mol L-1. A volume of 36.78 mL of sodium hydroxide is used to titrate each sample. The standard deviation of the burette used is 0.02 mL. Calculate the percentage of acetic acid in the vinegar and its standard deviation.Method used was Volhard Method Sample preparation: 5ml sample diluted in 100 ml. 20ml aliquot was used for analysis. Concentration of AgNO3: 0.0609M Calculate mass of NaCl and % NaCl (w/v)An unknown food-dye is analyzed by the method used in this experiment. The absorbance of 5 standard solutions is plotted vs. their concentration (molarity) and a straight line is obtained with the formula: Abs = 3.350x +0.08 An unknown food-dye soluton is diluted and it's absorbance is found to be 0.50. What is the molarity of the diluted unknown, to two significant figures?
- Standardization of Sodium Thiosulfate Solution Primary Standard used: Potassium Dichromate Formula mass of 1o standard: __________________ % Purity of 1o standard: 99.80% Trials 1 2 3 Weight of K2Cr2O7 (g)Weight of K2Cr2O7 (g) 0.0315 0.0331 0.0380 Final Volume Reading Na2S2O3 (ml) 27.50 27.50 34.90 Initial Volume Reading Na2S2O3 (ml) 1.10 0.00 1.00 Net Volume Na2S2O3 used (ml) Molarity of Na2S2O31. What is the MW of the analyte?2. What is the meq of the analyte?3. What will be the weight (in grams) of the analyte if the standardization is to be quartered?4. What will be Normality of the solution if 7.5ml of the titrant was consumed in the standardization?5. What is the average Normality if two or more trials were conducted with the values of 0.102N and 0.105N?An analysis of city drinking water for total hardness was done by two students in the laboratory and produced the following results (in ppm CaCO3): Student A: 228.3, 226.4, 226.9, 227.1, and 228.6. Student B: 229.5, 226.1, 230.7, 223.8, and 227.5 what is the coefficient variation?
- 1.50 mL of 0.15M Fe2(SO4)3 is diluted with deionized water to 25.00 mL in a volumetric flask. What is the concentration (in mg/mL) of iron (not Fe2(SO4)3) in the diluted sample? Please note that the units in this question are different than presented in the lab manual to avoid issues with exponents in a numerical answer. Of course if the units were in micrograms/g the results would be * 103 or (1000 times bigger).Measure the mass of 0.400g of Co(NO3)2 + 6H2O and dissolve it in 15mL of distilled or deionized water using a clean beaker Then while using a graduated cylinder, measure out 10.0mL of a prepared 0.10-M Na3PO4 soultion. Determine which compound Na3PO4 or Co(NO3)2 *6H2O will be the limliting reagent. Then detrimine the theiretical yeildJake carried out three titrations to determine the concentration of unknown nitric acid (HNO3) using 0.1050 M NaOH. He titrated 100.0 mL of the nitric acid sample and obtained the following volumes of NaOH: 20.56, 20.48, and 20.52 mL. The acid-base reaction occurring is NaOH (aq) + HNO3(aq) →→ NaNO3(aq) + H2O(l) Determine the concentration of the acid; report the average molarity with standard deviation. Pay attention to the number of significant figures on the mean and the number of decimal places on the standard deviation.