A student tries to synthesize ethyl acetate from 25 g glacial acetic acid (60.05 g/mol), 5 ml H2SO4 (98.08 g/mol), and 30 ml Ethanol (MW: 46.07 g/mol), d: 0,789 g/ml). After purification and drying process, 30 g Etyhl Acetate (88.11 g/mol) was obtained. Calculate the percent yield of the experiment. which one is the yield? calculate and show all the steps 66 % 83 % 81 % 68 %

A student tries to synthesize ethyl acetate from 25 g glacial acetic acid (60.05 g/mol), 5 ml H2SO4 (98.08 g/mol), and 30 ml Ethanol (MW: 46.07 g/mol), d: 0,789 g/ml). After purification and drying process, 30 g Etyhl Acetate (88.11 g/mol) was obtained. Calculate the percent yield of the experiment. which one is the yield? calculate and show all the steps 66 % 83 % 81 % 68 %

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter7: Extraction

Section: Chapter Questions

Problem 1Q

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A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted sample is transferred to the flask with a pipette, excess KI is added to it, and thus OCl- ion turns into Cl- ion and I2 is formed. The released iodine is titrated with 0.09892 Na2S2O3 using the starch reagent, and 8.96 mL is required for the endpoint. Find the % NaOCl (w/v; w/v) in the bleach sample. (Na=23 g/mol, O= 16 g/mol, Cl = 35.44 g/mol) (Warning: solving the necessary reaction equations by writing is necessary to see the stoichiometric relationship)
IDENTIFICATION: Acetylsalicylic acid commonly known as Aspirin (C9H8O4) is used to treat fever, inflammation, and acts as a blood-thinning agent. A group of STEM students experimented on the synthesis of this compound using recrystallization technique. The following are the initial materials for the experiment: 5.00 g of pure salicylic acid (C7H6O3), 7.14 g of acetic anhydride (C4H6O3) and 8 drops concentrated sulfuric acid as catalyst. After successful synthesis, the group was able to collect 5.25 grams of Aspirin (C9H8O4) and acetic acid (C2H4O2). Atomic weights: C= 12 amu; H = 1 amu; O= 16 amu; density acetic anhydride = 1.08 g/mL How much of the excess reactant (in grams) will be left unconsumed after the reaction?
5.0 mL of 1-butanol was mixed with 10 mL of HCl. The reaction was put on an ice bath and 4 mL of concentrated sulfuric acid was added. This mixture was refluxed for 45 min and then the product was co-distilled with water using a simple distillation apparatus. Water and the product are immiscible. 1-butanol has a molar mass of 74.12 g/mol, a density of 0.810 g/mL, and a boiling point of 118 C. The product has a molar mass of 92.57 g/mol, a density of 0.880 g/mL, and a boiling point of 78 C. What is the nucleophile in this reaction? What is the role of H2SO4 in this reaction? Calculate the theoretical yield for this reaction. Give your answer in grams. Select the following statements that can be said about the reaction shown.
A 0.9134-g of KIO3 is dissolved in 500-mL distilled water. A 50.0-mL aliquot portion was run down into an Erlenmeyer flask and 2-g of KI and 2-mL of 6M HCl were added to it. Directly after, the solution was titrated with a 24.47-mL Na2S2O3 solution to a faint yellow solution. Starch TS was added to the resulting solution and the titration with the Na2S2O3 solution continued wherein an additional 1.33-mL was required to bring the blue color of the solution to disappear completely. MW: KIO3 = 214.0 g/mol ; Na2S2O3 = 158.1 g/mol Compute the M of the Na2S2O3 solution. 0.1047 M None of the choices 0.1107 M 0.09926 M
A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted sample is transferred to the flask with a pipette, excess KI is added to it, and thus OCl- ion turns into Cl- ion and I2 is formed. The released iodine is titrated with 0.09892 M Na2S2O3 using the starch reagent, and 8.96 mL is required for the endpoint. Find the % NaOCl (w/v; w/v) in the bleach sample. (Na=23 g/mol, O= 16 g/mol, Cl = 35.44 g/mol) (Warning: solving the necessary reaction equations by writing is necessary to see the stoichiometric relationship) A. 0.132% B. 0.264% C. 5.28% D. 10.56%
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To synthesize methyl 3-nitrobenzoate, 20 ml of H2SO4 and 10 g of methyl benzoate were used. The nitrating mixture was prepared using 6 ml of H2SO4 and 6 ml of HNO3. Calculate the molar ratio of sulfuric acid to nitric acid
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19- A 25 mL liquid bleach sample is diluted with water to 1000 mL in a bubble gel. 25 mL of the diluted sample is transferred to the flask with a pipette, excess KI is added to it, and thus OCl- ion turns into Cl- ion and I2 is formed. The released iodine is titrated with 0.09892 M Na2S2O3 using the starch reagent, and 8.96 mL is required for the endpoint. Find the % NaOCl (w/v; w/v) in the bleach sample. (Na=23 g/mol, O= 16 g/mol, Cl = 35,44 g/mol)
A tea bag containing 15 grams of tea leaves with 0.7% of caffeine was used in solid-liquid extraction with 200ml of distilled water followed by liquid-liquid extraction using DCM. If 50.0mg of caffeine requires 10 ml of water and 3.0ml of DCM to be dissolved, how much caffeine can be extracted using 70.0ml of DCM? a. 4.8 x 10^-2 b. 5.7 x 10^-2 c. 3.8 x 10^-3 d. 5.8 x 10^-3
How to calculate grams of aluminum chloride using 2AI + 6HCI -> 2AICI3 + 3 H2 formed with 135 g of AI (with excess hydrochloric acid)?
In a Grignard reaction, 1.4555 g phenyl bromide, 10. g carbon dioxide, 0.5734 g magnesium filings, and 30.2 mL of 6M HCl were used but only 573 mg of benzoic acid were isolated after recrystallization? what was the percent yield for the overall process? Give the answer to the nearest whole number please