Compounds  Mass  3-nitrophthalic acid used 200 mg = 0.2g 8% aqueous hydrazine used  0.4mL 3-nitrophthalhydrazide obtained  130 mg = 0.13 g  sodium hydrosulfite dihydrate 0.6 g luminol obtained 70 mg = 0.07 g compute yield for nitrophthalhydrazide in the first step (assume nitrophthalic acid is limiting reagent) compute yield for luminol in the second step (using nitrophthalhydrazide as limiting reagent)  compute yield for the overall reaction

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter13: Isolation Of Eugenol From Clov
Section: Chapter Questions
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Compounds 

Mass 

3-nitrophthalic acid used

200 mg = 0.2g

8% aqueous hydrazine used 

0.4mL

3-nitrophthalhydrazide obtained 

130 mg = 0.13 g 

sodium hydrosulfite dihydrate

0.6 g

luminol obtained

70 mg = 0.07 g

compute yield for nitrophthalhydrazide in the first step (assume nitrophthalic acid is limiting reagent)

compute yield for luminol in the second step (using nitrophthalhydrazide as limiting reagent) 

compute yield for the overall reaction

 

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