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Solve this gravimetric analysis problem.
644 mg of a sample contains Mg (AW = 24) has been dissolved in water. The magnesium content of the sample is precipitated as MgNH4PO4.6H20 and ignited and weighted as Mg2P2O7 (mw= 222). If this weight is 290 mg, calculate the percentage of Mg in the sample?
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- detailed calculations on how to prepare the solutions listed below, Solution 1) 25 mL 7 M sulfuric acid and the respective dilution of this solution to prepare 50 mL 2 M sulfuric acid in deionised water. Sulfuric acid Mw = 98.079 g mol-1 Sulfuric acid density = 1.84 g mL-1 Sulfuric acid purity = 98%A chemist received different mixtures for analysis with the statement that they contained NaOH, NaHCO3, Na2CO3, or compatible mixtures of these substances, together with inert material. From the data given, identify the respective materials, and calculate the percentage of each component. 1.000g samples and 0.2500N HCl were used in all cases. (A) For Sample W: With PP, 24.32ml was used. A duplicate sample required 48.64ml with MO. (B). For Sample X: The addition of PP caused no color change. With MO, 38.47ml of the acid was required. (C). For Sample Y: To cause a color change in the cold with PP, 15.29ml of the acid was necessary, and an additional 33.19ml was required for complete neutralization. (D) For Sample Z: The sample was titrated with acid until the pink of PP disappeared; this process required 39.96ml. On adding an excess of the acid, boiling, and titrating back with alkali, it was found that the alkali was exactly equivalent to the excess acid added.If to a solution of NaOH, in water and ethanol (20 ° C) 3 mmol of A (106.11 g / mol) and 2 mmol of B (58.06 g/ mol) and stirred magnetically for 10 minutes. After the reaction is completed, we proceed to isolate (work- up) and purify at C (246.29 g/ mol) yielding 0.300 g of the pure product. Calculate the% return for C showing his work. please show every single step and calculations
- The %purity of a powdered crude sample of Na2CO3 containing only inert impurities is to be determined by reacting 225.0 mg of the crude sample to 10.0 mL of 3.00 M HCl solution, and bubbling the resulting CO2(g) product in water that is at exactly 29 °C. After the reaction has completed, the level of the liquid inside the eudiometer rests 4.30 cm above the water level in the beaker. The graduation on the eudiometer indicates that the trapped gas is 44.37 mL. The experiment was done under a barometric pressure of 755.2 torr. a. How many moles of CO2 were collected? b. What is the percent purity of the sample? Round off to the nearest whole numberThe %purity of a powdered crude sample of Na2CO3 containing only inert impurities is to be determined by reacting 225.0 mg of the crude sample to 10.0 mL of 3.00 M HCl solution, and bubbling the resulting CO2(g) product in water that is at exactly 29 °C. After the reaction has completed, the level of the liquid inside the eudiometer rests 4.30 cm above the water level in the beaker. The graduation on the eudiometer indicates that the trapped gas is 44.37 mL. The experiment was done under a barometric pressure of 755.2 torr. What CASE does this experiment satisfy?The concentration of purified OXA-M290 is tested with a BCA assay. Serial dilutions of a bovine serum albumin (BSA) stock solution are prepared, then pipetted into a 96-well plate; each dilution of the BSA standard is tested in triplicate. Then, bicinchoninic acid and Cu2+ ions are added to all of the wells of the plate. After incubating the plate for 1 hour, a microplate reader is used to measure the absorbance of all of the wells in the plate at 560 nm. This generates the following data: BSA conc. (μg/mL), Replicate 1 Absorbance, Replicate 2 Absorbance, Replicate 3 Absorbance 40, 1.360, 1.403, 1.481 20, 0.750, 0.745, 0.810 10, 0.380, 0.344, 0.398 5, 0.198, 0.160, 0.183 2.5, 0.090, 0.100, 0.085 1.25, 0.038, 0.043, 0.051 0.625, 0.024, 0.028, 0.019 Prepare a calibration curve using these data. You can use Excel, R, SPSS or an equivalent graphing software. In this graph, plot absorbance (y-axis) against the concentration of the protein standard (x-axis). Calculate and plot…
- Here is a use objective for a chemical analysis to be performed at a drinking water purification plant: “Data and results collected quarterly shall be used to determine whether the concentrations of haloacetates in the treated water demonstrate compliance with the levels set by the Stage 1 Disinfection By-products Rule using Method 552.2” (a specification that sets precision, accuracy, and other requirements). Which one of the following questions best summarizes the meaning of the use objective?(i) Are haloacetate concentrations known within specified precision and accuracy?(ii) Are any haloacetates detectable in the water?(iii) Do any haloacetate concentrations exceed the regulatory limit?detailed calculations on preparing the solutions listed below 25 mL of 0.1 M Cu(NO3)2 solution in deionised water 25 mL of 0.2 M Cu(NO3)2 solution in deionised water 25 mL of 0.5 M Cu(NO3)2 solution in deionised water 50 mL of 1.0 M HCl solution in deionised water Copper nitrate trihydrate: Formula: Cu(NO3)2.3H2O Mw: 241.60 g/mol State at RT: solid Purity: 98% Hydrochloric acid: Formula: HCl Mw: 36.46 g/mol State at RT: liquid Density: 1.18 g/ml Purity: 37% Acetic acid:The % purity of a powdered crude sample of Na^2CO^3 containing only inert impurities is to be determined by reacting 225.0 mg of the crude sample to 10.0 mL of 3.00 M HCl solution, and bubbling the resulting CO2(g) product in water that is at exactly 29 °C. After the reaction has completed, the level of the liquid inside the eudiometer rests 4.30 cm above the water level in the beaker. The graduation on the eudiometer indicates that the trapped gas is 44.37 mL. The experiment was done under a barometric pressure of 755.2 torr. Write the balanced chemical equation of the reaction in your solutions sheet. What is the sum of all the coefficients of the balanced chemical equation? Determine the pressure of the trapped gas inside the eudiometer in mmHg. Determine the partial pressure of the collected CO^2 in mm Hg. How many millimoles of CO^2 was collected? What is the % purity of the sample to the nearest whole number?
- The % purity of a powdered crude sample of Na^2CO^3 containing only inert impurities is to be determined by reacting 225.0 mg of the crude sample to 10.0 mL of 3.00 M HCl solution, and bubbling the resulting CO2(g) product in water that is at exactly 29 °C. After the reaction has completed, the level of the liquid inside the eudiometer rests 4.30 cm above the water level in the beaker. The graduation on the eudiometer indicates that the trapped gas is 44.37 mL. The experiment was done under a barometric pressure of 755.2 torr. What is the % purity of the sample to the nearest whole number?A empty evaporating dish weighs 30.56g. You place 20.0mL of an NaCl solution in the dish plus the solution weighs 53.31g. You evaporatorate the solution to dryness ant find that the evaporatoring dish plus the residue weighs 32.25g. What is the w/v%? What is the w/w%? What is the molarity?The standard addition method is used to analyze a sample of a river water for mercury. Solution A is made by pipetting 5.00 mL of undiluted sample in to a 10 mL volumetric flask and filling to the mark with DI water. Solution B is made by pipetting 5.00 mL of undiluted sample and 3.00 mL of 15.0 ppb of Hg standard into same 10.0 mL volumetric flask and filling to the mark with DI. Solution A and B are analyzed using atomic absorption spectroscopy and give a percent transmittance values of 56 % and 33 % respectively (not blank corrected). A blank has a transmittance of 96%. What is the corrected absorbance of both solution A and B? A. Solution A: 0.123 Solution B: 0.463 B. Solution A: 0.463 Solution B: 0.234 C. Solution A: 0.123 Solution B: 0.234 D. Solution A: 0.234 Solution B: 0.463