Spectra (Infrared in KBr, 'H-NMR in DMSO-d6, 400 MHz) LOD D 4D00 3000 2000 1500 1000 500 HAVENUMB ERI -l 3088 68 2667 70 1438 66 1142 81 793 745 74 3054 57 1694 1411 49 L125 84 12

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter8: An Introduction To Optical Atomic Spectrometry
Section: Chapter Questions
Problem 8.2QAP
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Question

 infrared data for the product in a table based on the data below 

experimental wavelength, peaks characteristics, assignment

Spectra (Infrared in KBr, 'H-NMR in DMSO-d6, 400 MHz)
LOD
D
4000
3000
2000
1500
000T
500
HAVENUMB ERI -||
3088
66
2667
70
1438
66
1142
a1
793
74
D691
1593
50
3054
57
1411
49
1125
84
745
12
2973
55
1318
19
1052
39
712
Б4
OH
2808
67
1671
6B
1200
67
1046
47
686
79
2825
60
1480
62
1268
41
956
79
648
64
2885
1475
64
1173
79
916
58
560
70
2663
62
1446
66
1161
84
816
78
480
B6
CI
TRANSMETTANCEIX!
Transcribed Image Text:Spectra (Infrared in KBr, 'H-NMR in DMSO-d6, 400 MHz) LOD D 4000 3000 2000 1500 000T 500 HAVENUMB ERI -|| 3088 66 2667 70 1438 66 1142 a1 793 74 D691 1593 50 3054 57 1411 49 1125 84 745 12 2973 55 1318 19 1052 39 712 Б4 OH 2808 67 1671 6B 1200 67 1046 47 686 79 2825 60 1480 62 1268 41 956 79 648 64 2885 1475 64 1173 79 916 58 560 70 2663 62 1446 66 1161 84 816 78 480 B6 CI TRANSMETTANCEIX!
14
12
10
6
4
2
HSP-41-134
ppm
Chemical Shift
Integration
Multiplet
13.43
1
S
7.81
1
d
7.56
1
d
7.55
1
7.45
1
t
00
Transcribed Image Text:14 12 10 6 4 2 HSP-41-134 ppm Chemical Shift Integration Multiplet 13.43 1 S 7.81 1 d 7.56 1 d 7.55 1 7.45 1 t 00
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