The gravimetric determination of Ni-t: Ni (58.7 g/mol) was precipitated as NIDMC) , (288.7 g/mol). The volume of unknown solution in the sample =15.00 mL. The mass of empty crucible = 30.107 g, the mass of empty crucible and precipitate = 30.300 g. Calculate the concentration of Ni-t in the unknown in sample solution (in mg/L) is: 1 02.62X103 2. 05.63X 103 3. O25.3X 104 4. 00.5X 10
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- The amount of sulfate in a solid sample was determined by first dissolving 562.2 mg of sample in water, and then precipitating the sulfate by the addition of 25.00 mL of 0.022 96 M BaCl2. The precipitate was filtered from the solution and the remaining Ba2+ was titrated with 16.52 mL of 0.014 57 M EDTA. What was the mass percent of sulfate in the solid?The arsenic in a 1.010 g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and exactly 40.00 mL of 0.06222M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag in the filtrate and in the washings from theprecipitate was titrated with 10.76 mL of 0.1000MKSCN; the reaction wasAg+ + SCN-→ AgSCN(s) Calculate the percent AsO3 in the sample.The solubility of borax, which is made up of sodium tetraborate (Na2B4O5(OH)4 8H2O), was analyzed. The dissolution of borax is: Na2B4O5(OH)4 • 8H2O(s) ⇌ 2 Na+(aq) + B4O5(OH)42–(aq) + 8 H2O(l) A 50 mL saturated solution was prepared. After filtration of solution, 5 mL aliquot was transferred to a flask and titrated using 0.432 M HCl. The endpoint was found to be 4.73 mL of the titrant. Tetraborate anion (B4O5(OH)42-) is a weak base which reacts with HCl like the following reaction: B4O5(OH)42–(aq) + 2 H+(aq) + 3 H2O(l) ⇌ 4 H3BO3(aq) What is Ksp expression for the dissolution? What is the tetraborate ions concentration in the filtrate? What is the molar solubility and Ksp of borax if the titration was done at room temperature (298 K)?
- The arsenic in a 1.223-g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, as 40.00 mL 0.07891 M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag+ in the filtrate and washings from the precipitate was titrated with 11.27 mL of 0.1000 M KSCN; the reaction was Ag+ + SCN- → AgSCN(s) Calculate the percent As2O3 in the sample.When standardizing two liters of a potassium permanganate solution, approximately 0.0100 M, with a primary standard solution of sodium oxalate, it was planned to use between 30.00 and 45.00 ml of the titrated reagent. In which mass range (in grams) the primary standard should be weighed?A sample containing calcium was analyzed by gravimetry, converting all calcium to calcium oxalate monohydrate (CaC2O4 • H2O). The sample weighing 0.2654 g was dissolved by adding 6M HCl, and then ammonium oxalate solution was added to precipitate all the calcium. The precipitate was suction filtered and dried in an oven at 95 °C for one hour. The solid obtained weighed 0.3216 grams.Calculate:A) The percentage of CaCO3B) The percentage of Ca C) The percentage of CaO
- The arsenic in a 1.203-g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and 40.00 mL of 0.05871 M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag+ in the filtrate and in the washings from the precipitate was titrated with 9.63 mL of 0.1000 M KSCN, and the reaction was. Find the percentage of As2O3 in the sample.Rei and Akari, two vinegar enthusiasts, are each tasked to determine the aceticacid content of their respective vinegar concoctions by titration. First, a 1M-labeled KOH solution was standardized against the KHP (MW = 204.22 g/mol)standard that is 99.4% pure. In the process, 0.540 g KHP was found to require2.80 mL of the KOH solution to completely react up to the phenolphthaleinendpoint. Then, Rei and Akari both prepared their samples by taking 10.0-mLaliquots of each vinegar and diluting them to 25.0 mL. Using the same titrant andindicator, Rei’s vinegar required 18.60 mL of the standardized titrant to reach theendpoint, while Akari’s vinegar required 16.50 mL of the same titrant to reach thesame endpoint. What is the exact concentration of the KOH titrant in molarity? What is the balanced chemical equation between the analyte and the titrant? What is the color transition (color X color Y) expected throughout thecourse of titration? What is the acetic acid concentration of Rei’s and…A solid sample containing some Fe2+ion had a total mass of .9791 g. It required 18.2 ml of 0.02304 M KMnO4 to titrate the Fe2+ in the dissolved sample to a pink endpoint. How many moles of Fe2+ were in the the sample? How many grams of irion were present in the sample and what was the mass percent iron in the sample?
- TOPIC: GRAVIMETRY SHOW THE SOLUTION The mercury in a 0.7152-g sample was precipitated with an excess of paraperiodic acid, H5IO6, according to the following reactions:5 Hg+2 + 2 H5IO6 ---> Hg5(IO6)2(s) + 10 H+The precipitate was filtered, washed free of precipitating agent, dried and found to weigh 0.3408-g. Calculate the percentage of Hg2Cl2 in the sample. Molar Masses: Hg5(IO6)2 = 1448.75 Hg2Cl2 = 472.09 Answer: 38.82% Hg2Cl2 An iron ore was analyzed by dissolving a 1.1324-g sample in concentrated HCl. The resulting solution was diluted with water, and the iron (III) was precipitated as the hydrous oxide Fe2O3·xH20 by the addition of NH3. After filtration and washing, the residue was ignited at a high temperature to give 0.5394 g of pure Fe2O3. Calculate (a) % Fe, and (b) % Fe3O4 in the sampleMolar Masses: Fe2O3 = 159.69 Fe = 55.847 Fe3O4 = 231.54 Answer: 33.32% Fe and 46.04% Fe3O4The concentration of CO in the air can be determined by passing a known volume of air through a tube containing I2O5, resulting in the formation of CO2 and I2. I2 is removed from the tube by distillation and collected in a solution containing excess KI, producing I3-. I3- is titrated with a standard solution of Na2S2O3. A 4.79 L air sample was sampled as described here, requiring 7.17 ml of 0.00329 M Na2S2O3 to reach the endpoint in a typical analysis. If the density of the air is 1.23×10^-3 g/ml, what is the amount of CO in the air in ppm? (CO: 28 g/ml)please help me The aluminum in a 1.200g sample of impure ammonium aluminum sulfate was precipitatedwith aqueous ammonia as the hydrous Al2O3 · XH2O. The precipitate was filtered and ignitedat 100°C to give anhydrous Al2O3, which weighed 0.2001 g. Express the result of this analysisin terms of % Al.