You have finished two trials of the sample analysis for the experiment and you noticed that the burette is almost empty (~5 mL remaining). Should you add more titrant before the next sample analysis or not? Why or why not? Select one: YES. It will not affect the calculations and not cause error NO. It will affect the calculations and cause error Neither A nor B Cannot be determined

You have finished two trials of the sample analysis for the experiment and you noticed that the burette is almost empty (~5 mL remaining). Should you add more titrant before the next sample analysis or not? Why or why not? Select one: YES. It will not affect the calculations and not cause error NO. It will affect the calculations and cause error Neither A nor B Cannot be determined

EBK A SMALL SCALE APPROACH TO ORGANIC L

4th Edition

ISBN:9781305446021

Author:Lampman

Publisher:Lampman

Chapter88: Column Chromatography

Section: Chapter Questions

Problem 5P

See similar textbooks

Similar questions

Can you proceed with sample analysis even without standardizing the titrant solution? Why or why not? You have finished two trials of the sample analysis for the experiment and you noticed that the burette is almost empty (~5 mL remaining). Should you add more titrant before the next sample analysis or not? Why or why not?
IF an analytical balance was not calbirated before gravimetry analyses, what will happen to the mass of final precipitate? Is it a Postive Error, Negative Error, No effect?
Calculate the mass percent of the ascorbic acid in the same show full solution Situation: The pounded Vitamin C tablet was half into two below are the calculated data in the experiment. Each of the half are transfered in a 250ml erlen meyer flask and added 75ml of deionized water for the vitamin C to dissolve. Then it was prepared for titration where the burette was filled with 0.09794M standardize NaOH solution then a total of with 3 drops 2% phenolphthalein indicator was added to each erlen meyer flask l, swrill it and begin the titration. below are the following data gathered: Vitamins used: Nature Made vitamin C 500mg tablet Trial 1 Mass: 0.3108g of Vitamin C tablet Initial volume: 1.6mL Final volume: 15.4mL Trial 2 Mass: 0.3349g Initial volume: 15.4 mL Final volume: 30.2 mL
A. A group of students are doing an analysis of copper in 1-peso coin. They were tasked to prepare standard solutions and weigh the analyte as the end-product of their experiment. Explain the type of error they are incurring in their experiment. A. Marikit had very good precision but poor accuracy in her data. B. Volumetric flasks were placed inside the oven for drying before it was used. C. Trial 1 and 2 have values close to 30.0 mL while trial 3 gave 55.0 mL. D. The reagent used in determining copper was added incorrectly and gave a low yield.
(Topic: Gravimetry multi-component analysis) The calcium and magnesium in a urine sample were precipitated as oxalates. A mixed precipitate of calcium oxalate and magnesium oxalate resulted and was analyzed by a thermogravimetric procedure. The precipitate mixture was heated to form calcium carbonate and magnesium oxide. This second mixture weighed 0.2504 g. After ignition to form calcium oxide and magnesium oxide, the resulting solid weighed 0.1563 g. What was the mass % of Ca in the mixed oxalate precipitate?
Am I calculating this correctly? Single 10 mL Extraction and Determination of Distribution Coefficient 1) Calculation of initial amount of benzoic acid in grams Volume of benzoic acid solution: 50.00 mL Molarity of benzoic acid solution: 0.0205 M 50.00 mL x 1 L/1000 mL L x 0.0205 mol/L x 122.122 g/mol = 0.12517505 g ≈ 0.125 g of benzoic acid A2. Calculation of amount of benzoic acid (g) remaining in aqueous solution after extraction with 10 mL of methylene chloride BA + NaOH --> sodium benzoate + H2O BA = 0.0205 M NaOH = 0.0189 M NaOH volume used = 17.4 mL Moles of NaOH: 0.0189 mol/L x 17.4 mL x 1L/1000 mL = 0.00032886 moles of NaOH BA:NaOH = 1:1, therefore there is 0.00032886 moles of BA remaining in aqueous phase 0.00032886 moles BA x 122.122 g/mol = 0.04016106 g 0.12517505 g BA (original) - 0.04016106 g BA (remaining) = 0.08158944 g BA in 10 mL of dichloromethane If everything is done correctly, how would I calculate of the amount of benzoic acid (g) extracted into the…
Following the monograph procedure, determine the weight in grams of sodium carbonate (MW-106 g/mol) used to standardize a 0.987 N sulfuric acid solution. 1. Consider that the burette was completely filled to the 0 mL mark before titrating. What is the volume of titrant consumed based from the image below? A. 22.9 mL B. 21.2 mL C. 21.3 mL D. 22.7 mL 2. What is the unknown weight (grams) in the problem? Your Answer:
If an instrument gives a response of 1240 for a standard containing 8 ppm of a substance, how much if this substance is in a sample that gives a response of 1705? Are any assumptions needed?
Which method of analysis generally is the faster method, gravimetric or volumetric? Why is that?
Scientist 1 analyzed the compounds first then gave it to scientist 2 for the next test. Scientist 2 needs to know the molar mass of the active compound. The concentration of the solution they created is twenty percentw/w from the solid active compound and it has a density of 1.40 grams per millilitre. Ten microliters were taken from this solution and mixed with one hundred ninety microliters of reagent and water. After analyzation, it showed that the compound's concentration is Five times ten raised to negative four M i. Find the concentration of the twenty percentw/w solution. The concentration must be in the form of molarityii. Explain the reason why the concentration of the solution was expressed as %w/w initially?iii. Determine the active compound's molar mass.
What are the types of gravimetric methods? Give an examples where each method is used in an analysis.
In a similar experiment, the mass of 3 PB tablets was measured to be 3.1823 g. The tablets were crushed, and 2.9801 g of the powder was transferred to a beaker and reacted with HCl. After filtration, the filtrate was transferred to a 50-mL volumetric flask and diluted with water. 10.00 mL of this stock solution was combined with 0.2 M Na3PO4. The resulting precipitate weighed 0.2425 g after drying. What is the mass of BSS per tablet in mg?Round your answer to 1 decimal place.