Chem 106 Identification of an Acid Lab Report

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Washington State University *

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Course

106

Subject

Chemistry

Date

Dec 6, 2023

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pdf

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4

Uploaded by BrigadierTurkey3888

Identification of an Acid The objective of this laboratory experiment was to use the data we collected via pH probe and spectrophotometer to identify an unknown weak acid. Acid-base equilibrium occurs when weak acids and bases react. Weak acids only partially ionize, and equilibrium is reached once there is a balance of ionized and unionized acid. This is depicted using this symbol: A pH titration is a method of obtaining data required to create a weak acid titration curve. You add a solution of a base to a solution of a weak acid in increments, and record how much the pH increases each time as well as how much of the base solution caused the increase. This allows you to plot a line and observe where the big jumps occurred. Usually, the curve ends up being an ‘S’ shape, where there are two obvious large increases in pH before it flattens out again. The purpose of this is to determine the titration’s equivalence point and half- equivalence point. These values allow you to determine the acid’s pKa and Ka values, which in turn allows you to determine the identity of the unknown acid. Methods and Analytical Plan The data I needed to record was how the acid solution was made (which unknown, mass of unknown used, & volume of the volumetric flask I made it in), how I did the titrations (initial and final burette readings recorded for each solution) as well as what I titrated it with, and finally, the pH reading for each solution that was made. This data was then used to determine pKa values for the acid [by identifying the half-equivalence point], calculate the molar mass of the acid, and use this information to (finally) identify the acid itself.
Data and Calculations I made the acid solution using 0.805 grams of a solid unknown acid ( unknown #1 ). I dissolved the solid acid in DI water in a beaker, and then poured it into a 250 mL volumetric flask that was then filled to the line with more DI water. I transferred 10 mL of the acid solution to a 150 mL beaker via a pipette before adding an additional 50 mL of DI water, measured using a graduated cylinder. I titrated this acid solution with a 0.4219M NaOH solution. Volume NaOH added (mL) pH reading 0 2.17 0.2 2.32 0.19 2.5 0.96 3.46 1.7 5.16 0.43 5.59 0.39 5.98 0.94 6.92 3.85 10.77 0.47 11.24 0.25 11.49 0.23 11.72 0.19 11.91 0.2 12.11 0.2 12.31 0.2 12.51
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