Experiment 19 Lab Report

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Salt Lake Community College *

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2320

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Chemistry

Date

Dec 6, 2023

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docx

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6

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Experiment 19: Qualitative Organic Analysis Unknown 1 Valentina Espinosa Canon Laboratory Partner: Dagmawit Duresa Professor Memari September 26th, 2023
2 Espinosa Materials and Method. Refer to Memari, Behnoush. CHM 2211L - Broward College-Central. Available from: VitalSource Bookshelf, (5th Edition). Macmillan Higher Education, 2023. Results: Table 1: Raw Data TEST RESULTS H 2 O Unknown did not dissolve. HCl Unknown did not dissolve, solid at the bottom of the test was visible. NaOH Unknown dissolved. NaOCH 3 Bubbles were observed, and then the solution completely dissolved. Titration results Melting point was found between 156-157 degrees Celsius. 1. Trial #1 & #2 same result Number of moles of NaOH = (mL of base used) × (1/1000 mL) × (molarity of the base) Number of moles of NaOH = 17.3 mL × (1/1000 mL) × 0.1 M = 0.00173 moles Molar mass = (mass of sample in grams) / (number of moles of acid) Molar mass = (0.225 g) / (0.00173 moles) = 130.06 g/mol Moles of acid = Moles of NaOH (1:1 stoichiometry) = 0.00173 moles FW = Mass of acid / Moles of acid FW = 0.225 g / 0.00173 moles FW ≈ 130.06 g/mol Unknown #1 = Salicylic acid Discussion:
3 Espinosa The purpose of this experiment was to identify an unknown organic compound, which could be an aldehyde, ketone, or carboxylic acid. Numerous steps were involved in the identification process, such as determining the boiling point, performing solubility tests, and performing classification tests. In order to identify the unknown compound #1, we first needed to determine its boiling point. We observed a melting point range of 156-157 degrees Celsius for the unknown. In order to conduct the solubility study, different solvents and solutions were used to test the unknown's solubility. According to the results, neither water nor hydrochloric acid dissolved the unknown. Upon mixing NaOH and NaOCH3 solutions, bubbles appeared and the solution dissolved completely. A carboxylic acid functional group may be present based on these observations. FW was calculated by performing a neutralization equivalent experiment to confirm the presence of carboxylic acid functional groups. The unknown solution was dissolved in ethanol, titrated with 0.1 M sodium hydroxide using phenolphthalein as the indicator, and 17.3 mL of NaOH used were recorded. A titration was performed twice, and an average was used to calculate the results. According to the calculation, FW is approximately 130.06 grams/mole. According to the observed melting point range and the FW, salicylic acid was identified as the unknown. Conclusion:
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