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Bs&W Procedure

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SAMPLING PROCEDURE FOR API AND BS&W Prepared by Mopu Lab. Technologist; Kumar 1. SAMPLING FOR BOTH API AND BS&W 2. Plastic bottles must not be used for sampling as there is a risk of a build-up of static charge and the container cannot be earthed to ground. Crude oil samples can only be sampled into earthed steel sampling containers. Earth leads must be used to reduce the potential for static ignition 3. Gas monitors should be used where hydrocarbon gas may be evolved. 4. Wear appropriate PPE when carrying out sampling. 5. Open the sampling point and flush the sample line into an earthed waste container for as long as needed to ensure the pipe work is hot enough. 6. Collect at least 500ml of …show more content…

Stopper and invert 10 times. 1.5.5 In the case where the crude oil is very viscous and mixing of the solvent with the oil would be difficult, the solvent may be added to the centrifuge tubes first to facilitate mixing. 1.5.6 loosen the stoppers slightly and place the tubes in the water bath for at least 15 min maintained at 60± 3°C (140± 5°C).Secure the stoppers and again invert the tubes ten times to ensure uniform mixing of oil and the solvent. 1.5.6 Place the tubes inside the centrifuge, on opposite sides so as to ensure a balanced condition. Re-tighten the corks and spin for 10 min at a minimum relative centrifuge force of 600, calculated using equation below r/min =133√(rcf/d) Where r/min = revolution per minute rcf = relative centrifuge force d = diameter of swing measured between tips of opposite tubes when in rotating position, in mm 1.5.7 When the centrifuge comes to a stop, read and record the combined volume of water and sediment at the bottom of each tube (The measurement must be to the nearest 0.05ml from 0.1 to 1 –ml graduations, and to the nearest 0.1ml above 1-ml graduations. Below 0.1ml, estimate to the nearest 0.025ml). 1.5.8 Return the tubes to the centrifuge and spin for another 10min at the same rate. Repeat this until the combined volume of water and sediment remains constant for two consecutive

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