A mixture containing iodide is analyzed by the Volhard method. 0.6712 g of the sample is reacted with 50.00 mL of 0.05619 M AGNO3. The precipitate formed is removed by filtration and the excess Ag+ is back titrated with KSCN 0.05322 M, requiring 35.15 mL to reach the end point. Calculate the concentration of iodide in the sample in parts per million (mg/kg).

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter17: Complexation And Precipitation Reactions And Titrations
Section: Chapter Questions
Problem 17.35QAP
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A mixture containing iodide is analyzed by
the Volhard method. 0.6712 g of the sample
is reacted with 50.00 mL of 0.05619 M
AGNO3. The precipitate formed is removed
by filtration and the excess Ag+ is back
titrated with KSCN 0.05322 M, requiring
35.15 mL to reach the end point. Calculate
the concentration of iodide in the sample in
parts per million (mg/kg).
Transcribed Image Text:A mixture containing iodide is analyzed by the Volhard method. 0.6712 g of the sample is reacted with 50.00 mL of 0.05619 M AGNO3. The precipitate formed is removed by filtration and the excess Ag+ is back titrated with KSCN 0.05322 M, requiring 35.15 mL to reach the end point. Calculate the concentration of iodide in the sample in parts per million (mg/kg).
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