arsenic in a 1.010 g sample of pesticide was converted to H3ASO4 by appropriate means. The acid neutralized and the arsenate precipitated quantitatively as Ag3As04 with exactly 40.00 mL of 22 M AgNO3. 3Ag* + AsO4→ Ag3AsO4 xcess Ag* was titrated with SCN , requiring 10.76 mL of 0.1000 M KSCN; the reaction being: Ag* + SCN → A SCN(s). late the percentage of As2O3 (MM = 197.841 g/mol) in the original sample.
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- The arsenic in a 1.010 g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and exactly 40.00 mL of 0.06222M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag in the filtrate and in the washings from theprecipitate was titrated with 10.76 mL of 0.1000MKSCN; the reaction wasAg+ + SCN-→ AgSCN(s) Calculate the percent AsO3 in the sample.The arsenic in a 1.203-g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and 40.00 mL of 0.05871 M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag+ in the filtrate and in the washings from the precipitate was titrated with 9.63 mL of 0.1000 M KSCN, and the reaction was. Find the percentage of As2O3 in the sample.The level of dissolved oxygen in a water sample can be determined by the Winkler method. In a typical analysis, a 100.0-mL sample is made basic, and treated with a solution of MnSO4, resulting in the formation of MnO2. An excess of KI is added, and the solution is acidified, resulting in the formation of Mn2+ and I2. The liberated I2 is titrated with a solution of 0.00870 M Na2S2O3, requiring 8.90 mL to reach the starch indicator end point. Calculate the concentration of dissolved oxygen as parts per million of O2.
- The arsenic in a 1.223-g sample of a pesticide was converted to H3AsO4 by suitable treatment. The acid was then neutralized, and 40.00 mL 0.07891 M AgNO3 was added to precipitate the arsenic quantitatively as Ag3AsO4. The excess Ag+ in the filtrate and washings from the precipitate was titrated with 11.27 mL of 0.1000 M KSCN; the reaction was Ag+ + SCN- → AgSCN(s) Calculate the percent As2O3 in the sample.The protein content of wheat flour can be determined reasonably accurately by multiplying the percentage of nitrogen present by 5.7. A 2.06-g sample of flour was taken through a Kjeldahl procedure and the ammonia produced was distilled into a boric acid solution. If this solution required 34.70 mL of 0.174 N HCl for titration to the methyl red end point, what is the a) % Nitrogen and b) % protein in the flour? (Use 1:1 stoich ratio between N and HCl)The amount of sulfate in a solid sample was determined by first dissolving 562.2 mg of sample in water, and then precipitating the sulfate by the addition of 25.00 mL of 0.022 96 M BaCl2. The precipitate was filtered from the solution and the remaining Ba2+ was titrated with 16.52 mL of 0.014 57 M EDTA. What was the mass percent of sulfate in the solid?
- A mixture of NaBr, Nal and NaNO3 weighs 0.6500 g. With AgNO3, a precipitate of the two halides is obtained and is found to weigh 0.9390 g. When heated in a current of C2, the precipitate is converted entirely to AgCi weighing 0.6566 g. What is the %NaNO3 in the original sample?As part of a soil analysis on a plot of land, a scientist wants to determine the ammonium content using gravimetric analysis with sodium tetraphenylborate, Na+B(C6H5)4−. Unfortunately, the amount of potassium, which also precipitates with sodium tetraphenylborate, is non‑negligible and must be accounted for in the analysis. Assume that all potassium in the soil is present as K2CO3 and all ammonium is present as NH4Cl. A 5.095 g soil sample was dissolved to give 0.500 L of solution. A 150.0 mL aliquot was acidified and excess sodium tetraphenylborate was added to precipitate both K+ and NH4+ ions completely. B(C6H5)4-+K+⟶KB(C6H5)4(s) B(C6H5)4-+NH4+⟶NH4B(C6H5)4(s) The resulting precipitate amounted to 0.269 g. A new 300.0 mL aliquot of the original solution was made alkaline and heated to remove all of the NH4+ as NH3. The resulting solution was then acidified, and excess sodium tetraphenylborate was added to give 0.129 g of precipitate. Find the mass percentages of NH4Cl and…calculate the mass of Sn when 50 mL of a sample containing Sn2+ is titrated with 42.00 mL of 0.0150M MnO4- to reach endpoint
- The aluminum in 0.200 g impure aluminum sulfate ( the sample) was precipitated with aqueous NH3and the precipitate was filtered and ignited to 10000C to give anhydrous Al2O3 (the residue) which weighs 0.150 g. Calculate the %Al ( the %sfc) in the sample.A sample of soluble salt weighs 1.2 g and contains chloride, bromide and iodide. With AgNO3, a precipitate is obtained which weighs 0.4500 g. On heating this precipitate with Cl2 gas, the AgBr and AgI are converted to AgCl, and the precipitate then weighs 0.3300 g. A similar sample, when treated with palladous chloride, precipitates only PdI2, and this precipitate weighs 0.0900 grams. (*)Find the approximate percentage of chlorine, bromine and iodine in the sampleA sample containing calcium was analyzed by gravimetry, converting all calcium to calcium oxalate monohydrate (CaC2O4 • H2O). The sample weighing 0.2654 g was dissolved by adding 6M HCl, and then ammonium oxalate solution was added to precipitate all the calcium. The precipitate was suction filtered and dried in an oven at 95 °C for one hour. The solid obtained weighed 0.3216 grams.Calculate:A) The percentage of CaCO3B) The percentage of Ca C) The percentage of CaO