Table 1: Estimation of DO. burette Final SLNO Volume of water Initial sample (ml) burette Volume of NazS203 reading (ml) reading (ml) consumed (V2 ml) 100.0 0.0 7.4 7.4 1 100.0 7.4 14.8 7.4 2 100.0 14.8 22.1 7.3 3 Calculations: Normality of water sample: N¡Vi(water sample) =N2V2(N22S2O3) -x 7.4 40 N2 XV2 N1 = 1.85 x 10-3 v1 100 N1 = 1.85 x 10-3 %3D Amount of Dissolved oxygen in water sample: Amount of free chlorine in water sample= N1 × equivalent weight of oxygen = 1.85 x 10-3 x 8 g/L 3D 1.85 х 10-3 х 8х 103 рpm 14.8 РPM %3D Amount of free chlorine in water sample= 14.8 PPM

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.16QAP
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EXPERIMENT :Estimation of Dissolved Oxygen

I want Result & Analysis for this experiment includes Precautions

Observations:
Table 1: Estimation of DO.
SINO Volume of water Initial
sample (ml)
burette Final
burette Volume
of
NazS203
reading (ml)
reading (ml)
consumed (V2 ml)
100.0
0.0
7.4
7.4
1
100.0
7.4
14.8
7.4
2
100.0
14.8
22.1
7.3
Calculations:
Normality of water sample:
N¡V1(water sample) =N2V2(Na2S2O3)
1
N2 XV2
x 7.4
40
N1 =
1.85 x 10-3
V1
100
N1 = 1.85 x 10-3
Amount of Dissolved oxygen in water sample:
Amount of free chlorine in water sample= N1 x equivalent weight of oxygen
1.85 х 10-3 х 8 д/L
%3D
3D 1.85 х 10-3 х 8х 103 рpm
= 14.8 PPM
Amount of free chlorine in water sample= 14.8 PPM
3.
Transcribed Image Text:Observations: Table 1: Estimation of DO. SINO Volume of water Initial sample (ml) burette Final burette Volume of NazS203 reading (ml) reading (ml) consumed (V2 ml) 100.0 0.0 7.4 7.4 1 100.0 7.4 14.8 7.4 2 100.0 14.8 22.1 7.3 Calculations: Normality of water sample: N¡V1(water sample) =N2V2(Na2S2O3) 1 N2 XV2 x 7.4 40 N1 = 1.85 x 10-3 V1 100 N1 = 1.85 x 10-3 Amount of Dissolved oxygen in water sample: Amount of free chlorine in water sample= N1 x equivalent weight of oxygen 1.85 х 10-3 х 8 д/L %3D 3D 1.85 х 10-3 х 8х 103 рpm = 14.8 PPM Amount of free chlorine in water sample= 14.8 PPM 3.
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