Two different laboratories within a company further studied the morantel recovery percentage in shrimp when spiking with 10 ug/kg. The results from both labs are presented below. Shrimp Sample Laboratory 1 (ug/kg) Laboratory 2 (ug/kg) 108.82 113.36 2 101.59 107.47 3 102.17 109.01 a. A 4th shrimp sample was analyzed for morantel recovery percentage using laboratory 1. The result was 99.4%, can any of the data be thrown out using the Q and/or Tn test using the 95th percentile? b. Is there a statistical difference (90th percentile) between the two laboratories results in the study?
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- If an instrument gives a response of 1240 for a standard containing 8 ppm of a substance, how much if this substance is in a sample that gives a response of 1705? Are any assumptions needed?The gravimetric factor used to express CoCBr6·H20 in a sample that is finally weighed as PbClBr is choose below: FW PbClBr / 6 x FW CoCBr6·H20 FW CoCBr6·H20 / FW PbClBr FW CoCBr6·H20 / 6 x FW PbClBr 6 x FW PbClBr / FW CoCBr6·H20Standardization of Sodium Thiosulfate Solution Primary Standard used: Potassium Dichromate Formula mass of 1o standard: __________________ % Purity of 1o standard: 99.80% Trials 1 2 3 Weight of K2Cr2O7 (g)Weight of K2Cr2O7 (g) 0.0315 0.0331 0.0380 Final Volume Reading Na2S2O3 (ml) 27.50 27.50 34.90 Initial Volume Reading Na2S2O3 (ml) 1.10 0.00 1.00 Net Volume Na2S2O3 used (ml) Molarity of Na2S2O3
- The concentration of purified OXA-M290 is tested with a BCA assay. Serial dilutions of a bovine serum albumin (BSA) stock solution are prepared, then pipetted into a 96-well plate; each dilution of the BSA standard is tested in triplicate. Then, bicinchoninic acid and Cu2+ ions are added to all of the wells of the plate. After incubating the plate for 1 hour, a microplate reader is used to measure the absorbance of all of the wells in the plate at 560 nm. This generates the following data: BSA conc. (μg/mL), Replicate 1 Absorbance, Replicate 2 Absorbance, Replicate 3 Absorbance 40, 1.360, 1.403, 1.481 20, 0.750, 0.745, 0.810 10, 0.380, 0.344, 0.398 5, 0.198, 0.160, 0.183 2.5, 0.090, 0.100, 0.085 1.25, 0.038, 0.043, 0.051 0.625, 0.024, 0.028, 0.019 Prepare a calibration curve using these data. You can use Excel, R, SPSS or an equivalent graphing software. In this graph, plot absorbance (y-axis) against the concentration of the protein standard (x-axis). Calculate and plot…Often the analyst will compare known quantities of analyte to unknown quantities of the material to be analyzed. This may be done in one of three ways: -use calibration curves; use standard additions; or use internal standards. The method of standard additions would be used when A) the quantity of sample analyzed or the instrument response varies from run to run. B) the standard solutions and the unknown solution all have similar characteristics are unaffected by the other material in the sample. C) the sample composition is unknown or complex and affects the analytical signal.I would need help with these questions. The method referenced above was followed by a student and she got the following results: Caffeine Std. Conc. (ppm) Absorbance 100 1.806 50 0.899 40 0.724 30 0.545 20 0.365 10 0.183 Further, she analyzed an unknown sample and she got the following results: Sample # Absorbance 1 0.398 1. Graphically find the concentration in ppm and then calculate in mol/L of Caffeine in Sample #1? 2. Which solvent was used to extract Caffeine and why? Why is it necessary to do extraction three times? 3. Cuvettes used in this experiment were made from which material and why? 4. At what wavelength the Absorbance was measured?
- 125.1 mg of streptomycin sulphate are dissolved in 10 ml of water. A GC headspace analysis is carried out in order to determine the methanol content of the drug. A peak for methanol is produced which has 73.2% of the area of a peak for a methanol standard containing 0.532 mg/100 ml of methanol in water analysed under exactly the same conditions, What is the methanol content of the streptomycin sulphate in ppm and %w/w? Answer: 311.3 ppm, 0.3113 % w/w.how??Amylum, commonly known as starch is a white powder with variable molecular formula due to the different number of repeating sugar units based on the plant that it is obtained from. A sample of amylum in the form of spherical beads was subjected to series of analyses to determine physicochemical properties in the quality control unit of a factory. From the results each bead is found to have a 4.5 mL volume and 1.47 g/mL density. 4 of the beads were placed in a reaction chamber combusted, as a result, 43.1 g CO2 and 14.7 g H2O were obtained. If the molecular weight of the amylum is 972.84 g/mol how many repeating units the starch molecule consist and what is the molecular formula of the starch? [Empirical Formula=CxHyOz, Repeating unit=n, Molecular Formula=( CxHyOz)*n= CnxHnyOnz]50 mg of granular salt is briefly stirred into a glass container of 1/5 liter volume filled with water. After briefly mixing, some salt is still seen at the bottom of the class. The visible salt is filtered from the water, weighed and determined to have a mass of 20 mg. What is the dissolved phase concentration of salt remaining in the water? Provide your answer to the nearest whole number in units of mg/l.
- 1. You give your home health patient an unopened 500-mL bottle of guaifenesin and tellthem to take 2 teaspoons 4 times a day as ordered. They ask you how long the bottlewill last. 2. You are shadowing a nurse during a clinical who receives an order to adjust the infusionrate of a pump so that 1.6 mg of lidocaine are being delivered per minute. Hanging is a100 mL piggyback containing 0.4 grams lidocaine, a 0.4% solution. How many mL perhour should the piggyback be set to deliver? How long will the piggyback last? 3. Phenobarbital 180 mg/m 2 /24 hours given every eight hours is ordered for a childwhose BSA (body surface area) is 0.29 m 2 . How many mg will you need if the child willbe on the medication for 10 days? 4. You are going to mix a 1:10 bleach solution with water to make 500 mL of a 1:35 bleachsolution. How much 1:10 bleach solution should you use?(I recommend using the C1V1=C2V2 formula) 5. As a home health nurse you need to help a client make…Table of caffeine standards concentration . Sample Conc, ppm Std1 16 Std2 32 Std3 48 Std4 64 Std5 80 If the volume used to make 100 mL of std 1 is 2 uL what is the concentration in M used to make std calibration curve ? The standards are going to be used to build calibration curve to analyze caffeine in an energy drink. if 500 mL of the energy drink has target of 400 mg , how will you prepare the sample if you need 10 mL for the analysis ? Caffeine MM=194.19 g/mol.Calculate the Standardized Molarity of NaOH via dimensional analysis. Show your process.Use this table in answering the Standardized Molarity of NaOH in Trials 1, 2, and 3. TRIALS 1 2 3 Actual weight of Std. KHP (g) 0.8026 0.8032 0.8021 Corrected weight of KHP (g) based on % purity of primary std. 0.7986g 0.7992g 0.7981g Volume NaOH used (ml) 39.45 39.35 39.47