Which of the following is correct: Selection of the method is the first step in the qualitative analysis. Volume is the analytical signal in gravimetric method. Removal of interferences is not
Q: what parameters and quality control measures are needed in spectrophotometer?
A: The parameters and quality control measures are needed in spectrophotometer has to be given,
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Q: Describe how to use a spectrophotometer
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- a- Separation is essential in chemical analysis especially when we are dealing with complexmixture of chemical species. Name 1 separation technique based on basis of operation asbelow. Basis of operation Techniquei) Sizeii) Mass and densityiii) Change in physical statehree components in a mixture have varying distribution constants between the mobile phase and the stationary phass One of the components has a very low distribution constant, Would this component likely elute first or last and how would you design an experiment or modify the components of the separation to make it perform in the opposite manner?Anion and cation chromatography can be achieved by modifying? A. Type of dye B. Mobile phase C. Wavelength D. Stationary phase
- One method for the quantitative determination of the concentration of constituents in a sample analyzed by gas chromatography is area normalization. Here, complete elution of all the sample constituents is necessary. The area of each peak is then measured and corrected for differences in detector response to the different eluates. This correction involves dividing the area by an empirically determined correction factor. The concentration of the analyte is found from the ratio of its corrected area to the total corrected area of all peaks. For a chromatogram containing three peaks, the relative areas were found to be 16.4, 45.2 and 30.2, in order of increasing retention time. Calculate the percentage of each compound if the relative detector responses were 0.60, 0.78 and 0.88, respectively.Describe the following as used in analytical chemistry a) semiqualitative analysis b)Assay c) derivatisationA standard curve for glucose analysis was prepared.The slope (m) was found to be 1.341 while the y-intercept (b) was -0.333. Calculate the concentration (x) of glucose having an absorbance (y) of 0.151. 0.067 0.361 0.858 0.136
- A 0.1 M solution of acid was used to titrate 10 ml of 0.1 M solution of alkali and thefollowing volumes of acid were recorded: 9.88 10.18 10.23 10.39 10.21 Calculate the 95% confidence limits of the mean and use them to decide whetherthere is any evidence of systematic error.A 5.3 × 10-2 M solution is to be used to prepare a series of five 100 mL solutions of varying concentration for use in creating a calibration curve for a spectrophotometric experiment. Determine the concentrations of each of the five dilutions if 10 mL aliquots of the current solution is used for V1.A spectrophotometric method for the quantitative determination of the concentration ofPb2+ in blood yields an Ssamp of 0.133 for a 1 mL sample of blood that has been diluted to 6 mL. A second sample is spiked with 1 µL of a 1467 ppb Pb2+ standard and diluted to 6 mL, yielding an Sspike of 0.491. Determine the concentration of Pb2+ in the original sample of blood.
- A chemical species that causes a systematic error in an analysis by enhancing or attenuating the analytical signal or the background. A. Interferent B. Analyte C. Cation D. AnionThe following calibration data were obtained by an atomic absorption spectrophotometric (AAS) method for the determination of mercury in an herbal product. (show complete solution) 1. What is the detection limit for the method? 2. What is the limit of quantitation for the method?Two commonly used chromatography methods in labs are Nickel and streptavidin resin based colums. Explain which type of chromatography-ion exchange, size-exclusion, or affinity-these are, as well as their seperation mechanisms at a molecular level.