Lab Report 02 - Russell

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Drexel University *

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244

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Chemistry

Date

Feb 20, 2024

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pdf

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11

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Nalo Russell Experiment 2 - Distillation Fill in the blanks in the given template. Use underlines, boldface, or parentheses to clearly indicate the filled content within the context. Type up the report and save it as one single file in the PDF format. Submit the PDF file by the deadline. Key Observations Part A - Volume of methanol 13 mL in the distillation pot to distill. - Power of the heating mantle used during the distillation 40-50% . - Collected distillate: volume 10 mL , color clear , bp range 61° - 66 ° C. Part B - Volume of 50:50 methanol-water 13 mL in the distillation pot to distill. - Power of the heating mantle used during the distillation 50% . - Collected distillate: volume 10 mL , color clear , bp range 69° - 99° C. Part C - Volume of 50:50 methanol-water 13 mL in the distillation pot to distill. - Power of the heating mantle used during the distillation 50% . - Collected distillate: 10 mL - Fraction 1: volume 1 mL, bp range 66° C . - Fraction 2: volume 3 mL, bp range 68° - 80° C. - Fraction 3: volume 1 mL, bp range 87° C. - Fraction 4: volume 4 mL, bp range 92° - 98° C. - Fraction 5: volume 1 mL, bp range 98°C.
Results Insert graph 1: bp vs volume from part A. (An excel plot should occupy the majority of a properly scaled and labeled X-Y coordinate plane. All data points should be marked and connected with a trendline. Provide a title that gives a brief and clear description of the graph, and a caption that gives a more detailed description of the graph).
Insert graph 2: bp vs volume from parts B and C. (Combine both plots in the same coordinate plane. Follow the instructions for graph 1).
Attach a copy of each GC spectrum.
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