Lab Report 02 - Russell
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Chemistry
Date
Feb 20, 2024
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Nalo Russell
Experiment 2 - Distillation
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indicate the filled content within the context. Type up the report and save it as one single file in
the PDF format. Submit the PDF file by the deadline.
Key Observations
Part A
-
Volume of methanol
13
mL in the distillation pot to distill.
-
Power of the heating mantle used during the distillation
≅
40-50% .
-
Collected distillate: volume
10 mL , color
clear , bp range
61° - 66 ° C.
Part B
-
Volume of 50:50 methanol-water
13
mL in the distillation pot to distill.
-
Power of the heating mantle used during the distillation
≅
50% .
-
Collected distillate: volume
10 mL , color
clear , bp range
69° - 99° C.
Part C
-
Volume of 50:50 methanol-water
13
mL in the distillation pot to distill.
-
Power of the heating mantle used during the distillation
≅
50% .
-
Collected distillate: 10 mL
-
Fraction 1: volume
1 mL, bp range
66° C .
-
Fraction 2: volume
3
mL, bp range
68° - 80° C.
-
Fraction 3: volume
1
mL, bp range
87° C.
-
Fraction 4: volume
4
mL, bp range
92° - 98° C.
-
Fraction 5: volume
1
mL, bp range
98°C.
Results
Insert graph 1: bp vs volume from part A. (An excel plot should occupy the majority of a
properly scaled and labeled X-Y coordinate plane. All data points should be marked and
connected with a trendline. Provide a title that gives a brief and clear description of the graph,
and a caption that gives a more detailed description of the graph).
Insert graph 2: bp vs volume from parts B and C. (Combine both plots in the same coordinate
plane. Follow the instructions for graph 1).
Attach a copy of each GC spectrum.
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Related Questions
Unit 3-Two slides
11. Create a question that involves your compound and the formula m= n.M. Solve the question and show all of
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wwwww
12. Create a question that involves your compound and the formula n = N/NA. Solve the question and show all of
your work.
TE
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Methods of Analysis
Test #1: Polarity, or Effect of a charged rod on a stream of liquid:
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Try this at home with water and a plastic spoon. Rub the plastic spoon against a sweater and move it close to a small stream of water running out of your faucet!
Test #2: Volatility, or Rate of Evaporation:
A thermometer probe was wrapped with a strip of filter paper. This assembly was soaked in one of the liquids for one minute. The probe was removed, and the temperature change was monitored as the liquid evaporated. The results are given in Graph 1 below. (See Graph)
Graph 1: The curves generated of the change in temperature over time for the substances acetone, hydrogen monoxide, ethylene glycol,…
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terface/acellus_engine.htm?ClassID=1467683063
Use the data below to determine the
mass ratio of iron to oxygen for
compound 2.
Compound
1
2
Et
onal Academy of Science. All Rights Reserved.
Mass Fe
(grams)
15.55
20.98
[20:1
Enter the answer that belongs in the green box.
Iron Ratio Cmpd 2
Mass O
(grams)
4.45
9.02
Sh
Enter
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105 words
+ 396%
10:50 AM
O Type here to search
32°C Mostly sunny
W
4/23/2022
出
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student found a bottle of unknown origin in the basement of an
"CAUTION—contains С₁H₁O.” No other
A
old house. The bottle was labelled
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crystals with the help of the laboratory staff. C₁2H₁6O reacted with Br₂ in CCl4
adding one mole of Br, and forming C₁₂H₁OB2₂.
When a sample of C₁₂H₂O was reacted with O3 followed by Zn/H₂O, two
different samples, J and K, were obtained. Compound J had a molecular formula
of C.HgO₂, and its NMR is shown below.
Compound K had a molecular formula of C₂H₂O, and it could be oxidized to
compound L, with a molecular formula of C₂H₂O₂. The IR spectrum of L showed
a very wide, strong band centred around 3000 cm*¹. The NMR spectrum of L
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You were tasked to separate the components of a mixture containing silica, sodium chloride and charcoal. TNāCI
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a. Write a short experimental procedure to carry out the separation of the mixture.
b. Given the following data, determine the percentage of charcoal, sodium chloride and silica.
Mass (g)
Mass of beaker
100.000
Mass of beaker + mixture
110.000
mass of evaporating dish
62.000
mass of evaporating dish + solid after
evaporation of water
65.000
Mass of beaker + charcoal + silica after evaporation of
excess water
117.000
mass of beaker + silica after decanting dissolved charcoal
and drying
113.545
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solution. Follow up by running measurements on sample
solutions. Once data is collected, turn off the instrument, clean the area, and
discard the samples.
Partially correct
(2 of 4 correct)
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Which one is the most common method used for the purification of liquid mixtures?
Filtration
Chromatography
Evaporation
Distillation
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TV = 39.165%
EV = 40.767%
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00
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# 3.
5o09
awww.awu.aleks.com/alekscgi/x/Isl.exe/1o_u-IgNslkr7j8P3jH-lijulplKKWv4bwenmyrLYoBHBAAsJtmzj53GErnx_viTdHblGMF9jvgkSu_nrizREmdQXHPJbMzqOmOrXJcuonZITOhB66q?1oBw7QYlbav.
LEKS-Courtney Wh
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+ x
O CHEMICAL REACTIONS
Percent yield of chemical reactions
Courtney
S0 OC
Gaseous butane
CH.
reacts with gaseous oxygen gas (0,) to produce gaseous carbon dioxide (CO,) and gaseous water (H,0). If 2.32 g of
water is produced from the reaction of 1.74 g of butane and 10.2 g of oxygen gas, calculate the percent yield of water.
Be sure your answer has the correct number of significant digits in it.
%
固
Explanation
Check
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liquid-liquid
solid-liquid
solid-phase
Phase that contains analyte
before extraction?
Phase that contains analyte
after extraction?
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Summative Assessment
Summative:
Components of the Lab Report
Purpose: The student should clearly state the purpose of the experiment, which is to determine whether the mixing of two or more substances results in new substances.
Procedure: The student should describe the steps they took to conduct the experiment. This includes the substances they chose to mix and the safety equipment they used.
Observations: The student should record any observable changes that occurred when the substances were mixed. This could include a color change, the formation of a precipitate, or a change in temperature.
Conclusion: The student should state whether a new substance was formed based on their observations. They should also reflect on their accuracy in…
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1) Listen
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The Ksp value for calcium sulfate [CaSO4] is 2.40 X 10 and a professor made 1825
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the additional volume coming from the Ca3(PO4)2 solution to make the calculation
simpler. Calculate the new sulfate (SO42) ion concentration at equilibrium with this
common ion effect.
6.40 x 10-5
5.25 x 10-5
6.21 x 10-5
5.44 x 10-5
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Group of answer choices
True
False
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