Dissolve 1 g of acetaminophen d.s 30 to 40 mL of water. Add 1 mL of nitric acid plus 1 mL of silver nitrate TS, and sufficient water to make the final volume 50 mL. Mix, and allow to stand for 5 minutes protected from direct sunlight. Unless otherwise specified in the monograph, this mixture should not be more turbid than that produced when 1 mL of silver nitrate TS is added to a 50 mL standard solution containing 10 mL of 0.020 N hydrochloric acid. For the Limit of Chloride test, above, select the correct specification. A. Sample mixture should not be as turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid. B. Dissolve 1 g of acetaminophen d.s 30 to 40 mL of water. C. Sample mixture should not be more turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid. D. Sample mixture should not be more turbid than that produced by 1 mL of silver nitrate TS. E. Sample mixture should not be less turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid. F. Add 1 mL of nitric acid plus 1 mL of silver nitrate TS, and sufficient water to make the final volume 50 mL.

EBK A SMALL SCALE APPROACH TO ORGANIC L
4th Edition
ISBN:9781305446021
Author:Lampman
Publisher:Lampman
Chapter81: Extractions, Separations, And Drying Agents
Section: Chapter Questions
Problem 8P
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  1. Limit of CHLORIDE test 

    Dissolve 1 g of acetaminophen d.s 30 to 40 mL of water.

    Add 1 mL of nitric acid plus 1 mL of silver nitrate TS, and sufficient water to make the final volume 50 mL. Mix, and allow to stand for 5 minutes protected from direct sunlight.

     

    Unless otherwise specified in the monograph, this mixture should not be more turbid than that produced when 1 mL of silver nitrate TS is added to a 50 mL standard solution containing 10 mL of 0.020 N hydrochloric acid.

     

    For the Limit of Chloride test, above, select the correct specification.

      A.

    Sample mixture should not be as turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid.

      B.

    Dissolve 1 g of acetaminophen d.s 30 to 40 mL of water.

     

      C.

    Sample mixture should not be more turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid.

      D.

    Sample mixture should not be more turbid than that produced by 1 mL of silver nitrate TS.

      E.

    Sample mixture should not be less turbid than that produced when 1 mL of silver nitrate TS is added to a standard solution containing 10 mL of 0.020 N hydrochloric acid.

      F.

    Add 1 mL of nitric acid plus 1 mL of silver nitrate TS, and sufficient water to make the final volume 50 mL.

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