Principles of Instrumental Analysis
Principles of Instrumental Analysis
7th Edition
ISBN: 9781305577213
Author: Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher: Cengage Learning
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Chapter 14, Problem 14.2QAP

A 0.4740-g pesticide sample was decomposed by wet ashing and then diluted to 200.0 mL in a volumetric flask. The analysis was completed by treating aliquots of this solution as indicated.

Chapter 14, Problem 14.2QAP, A 0.4740-g pesticide sample was decomposed by wet ashing and then diluted to 200.0 mL in a

Calculate the percentage of copper in the sample.

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For the gravimetric determination of manganese, 1.8762 g of sample containing Mn was dissolved in acid solution and made up to 100 mL in a calibrated volumetric flask. A 25.00 mL aliquot of this solution was transferred to a beaker. The solution was heated to boiling and chemical substances required were added till precipitating MnNH4PO4. After filtering, rinsing, and igniting, 0.5365 g of Mn2P2O7 was obtained. Calculate the % manganese in the sample (Mn: 55, P: 31, O: 16 g/mol).
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