Macroscale and Microscale Organic Experiments
Macroscale and Microscale Organic Experiments
7th Edition
ISBN: 9781305577190
Author: Kenneth L. Williamson, Katherine M. Masters
Publisher: Brooks Cole
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Chapter 8, Problem 12Q
Interpretation Introduction

Interpretation:

The Rf value for substance B in figure 8.10 should be calculated.

Concept introduction:

The Rf value or the retention factor is defined as the ratio of distance traveled by the spots by the distance traveled by the solvent.

  Rf=Distance travelled by spotDistance travelled by solvent

The more the compounds move, the higher is the Rf value. Thus the polarity of the compound helps in deciding the Rf value.

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A student measured the melting point range of an unknown solid to be 72.4 to 78.6 degrees celsius. a) Is the compound pure? b) Can you identify the compound from Table 2.2? c) If yes, what is the compound? If no, what compounds from Table 2.2 can be excluded? Table 2.2: Solid - Melting Point (Celsius) Benzoic Acid - 122 Acentanilide - 114 Acetamide - 82 Biphenyl - 71 p-Dimethoxybenzene - 59 p-Dichlorobenzene - 54 Benzophenone - 48
A student measured the melting point range of an unknown solid to be 81.9 to 82.3 degrees celsius. a) Is the compound pure? b) Can you identify the compound from Table 2.2? c) If yes, what is the compound? Table 2.2: Solid - Melting Point (Celsius) Benzoic Acid - 122 Acentanilide - 114 Acetamide - 82 Biphenyl - 71 p-Dimethoxybenzene - 59 p-Dichlorobenzene - 54 Benzophenone - 48
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