Recrystallization Post-Assignment

Suppose that you have a 1:1 mixture of compounds that is comprised of compound X and compound Y. You desire pure compound X and are planning a recrystallization to enhance the purity. Which solvent below is optimal for your recrystallization?      Ethanol (boiling point = 78 °C)   Solubility At   0  °C 100  °C Compound X 0.05 g/mL 0.20 g/mL Compound Y 0.02 g/mL 0.40 g/mL           Water (boiling point = 100 °C)   Solubility At   0  °C 100  °C Compound X 0.02 g/mL 0.05 g/mL Compound Y 0.01 g/mL 0.10 g/mL           Methanol (boiling point = 65 °C)   Solubility At   0  °C 65  °C Compound X 0.04 g/mL 0.10 g/mL Compound Y 0.02 g/mL 0.30 g/mL         Acetone (boiling point = 56 °C)   Solubility At   0  °C 56  °C Compound X 0.10 g/mL 0.50 g/mL Compound Y 0.20 g/mL 0.50 g/mL         Ethyl Acetate (boiling point = 77 °C)   Solubility At   0  °C 77  °C Compound X 0.10 g/mL 0.60 g/mL Compound Y 0.30 g/mL 0.60…

The position of the phases in the separatory funnel (whether the top or bottom phase) is dependent on the relative densities of the solvents. Complete table 1 to indicate whether each of the solvents will be on the top or bottom layer. Table 1. Solubility properties of common organic solvents. Solubility in H20 (g/L, 20-25°C) 9.5 x 10-3 1.79 8.09 17.5 Solubility of H20 (g/L, 20-25°C) 0.31 Phase layer Density (g/mL, 25°C) 0.661 Liquid hexane benzene chloroform 0.76 0.87 1.76 15 170 0.877 dichloromethane diethyl ether 1-butanol 60.5 73 0.3 1.489 1.327 0.713 0.81 0.83 1-octanol 49 ethyl acetate 83 33 0.902

2. Questions: 1. CHM-202 Lab 2 Freezing Point Depression Rev2 G6-2022 10/14 From your understanding of colligative properties, how would you design an experiment to measure the freezing point of a material which freezes at -2 °C using the same apparatus used in this laboratory and any chemical reagents commonly found in a chemical laboratory. Ice is the only material you have available to cool the solutions. If you measured the boiling point of the solution used in Trial 4, would you predict it would have a boiling point equal to, higher than, or lower than the boiling point of pure cyclohexane? Explain your answer.

4. Why is fractional distillation more "efficient" than simple distillation? During boiling point determination the temperature of the vapors is be E

A certain liquid X has a normal boiling point of 93.90 °℃ and a boiling point elevation constant K₁ = 1.14 °C-kg-mol¯¹. Calculate the boiling point of a solution made of 40.1g of zinc chloride (ZnCl₂) dissolved in 350. g of X. Round you answer to 4 significant digits. °C x10 X 1 Ś

Cyclohexanol 10 ml Mass of cyclohexanol 9.62 g – 0.053 mol Theroretical yield  cyclohexene–7.89g - ? mol Therotical mass of cyclohexene- Actual yield- 6.8ml –4.055 g –? mol Percent yield- 51.04% Boiling point of cyclohexene -83 degree Celsius Theroretical boling point -83 degree Celsius can i get some clarification pls

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However, there are many other commercially purchased inorganic and organic compounds that people routinely used in their households (or in their everyday lives). A list of 19 chemicals with common names are written below. Find each of these items in your home or in a local grocery and take picture of the container (if you do not have access to all of them choose at least 12 of them) and then complete the table below. For #16 and 17 you choose any other house hold chemical and complete the table. • Inorganic compounds 1) table salt, 2) baking soda, 3) washing soda, 4) photographic fixer, 5) Epsom salt, 6) alum, 7) chalk, 8) corn starch, 9) sand, 10) active ingredient in toothpaste or cleansing agent and disinfectant, 11) decolorizing carbon Organic compounds Naming of organic compounds will be discussed in details in Lab 10 however there are still some simple organic compounds that you encounter at your home. Organic compounds are compounds that contain at least one carbon with one…

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Solutes have almost no effect on the boiling & freezing points of a solvent.  True  False

2. The table below has IUPAC names and boiling points for four of the organic compounds discussed in the Kahn Academy video on simple and fractional distillation. Draw the structure of each compound, and label the polar and nonpolar groups with the type of attractive force the molecules can use to interact with one another. acetone (2-propanone); boiling point = 56 °C Polar dipoit-dipole dispersion, nonpolar cyclohexane; boiling point = 81 °C 가~ -nonpolar, dispersion ethanol; boiling point = 78 °C Polar, hydrogen (OH) bonding nonpolar acetic acid (ethanoic acid); boiling point = 118 °C E polar, dipole-dipole honpolar, OH 7-polar, hydrogen bonding dispersion Explain the relative boiling points of these compounds in terms of the attractive forces and masses of each molecule.

In addition to the separation techniques used in this lab (magnetism, evaporation, and filtering), there are other commonly used separation techniques. Some of these techniques are:Distillation – this process is used to separate components that have significantly different boiling points. The solution is heated and the lower boiling point substance is vaporized first. The vapor can be collected and condensed and the component recovered as a pure liquid. If the temperature of the mixture is then raised, the next higher boiling component will come off and be collected. Eventually only non-volatile components will be left in the original solution.Centrifugation – a centrifuge will separate mixtures based on their mass. The mixture is placed in a centrifuge tube which is then spun at a high speed. Heavier components will settle at the bottom of the tube while lighter components will be at the top. This is the technique used to separate red blood cells from blood plasma.Sieving – this is…

ed The boiling point of water is 100.00 °C at 1 atmosphere. A student dissolves 12.63 grams of sodium sulfide, Na₂S (78.05 g/mol), in 163.3 grams of water. Use the table of boiling and freezing point constants to answer the questions below. Solvent Water Ethanol Chloroform Benzene Formula H₂O CH3CH₂OH CHCI 3 соно Diethyl ether CH3CH₂CH₂CH3 The molality of the solution is The boiling point of the solution is Kb (°C/m) Kf (°C/m) 0.512 1.86 1.22 1.99 3.67 2.53 2.02 m. °C. 5.12

Rank these substances in order of increasing solubility in water. Solubility Substances (4 items) (Drag and drop into the appropriate area) Most soluble CH3CH2CH2OH 1 CH3(CH2)5OH CH3(CH2)3OH 2 CH3CH2OH 3. 4 Least soluble

What is the classification of each substance

When 184. mg of a certain molecular compound X are dissolved in 85. g of formamide (NH,COH ), the freezing point of the solution is measured to be 1.7 °C. Calculate the molar mass of X. If you need any additional information on formamide, use only what you find in the ALEKS Data resource. Also, be sure your answer has a unit symbol, and is rounded to the correct number of significant digits. Ox10 미

A certain liquid X has a normal boiling point of 105.30 °C and a boiling point elevation constant K₁ = 1.74 °C-kg-mol¯¹. Calculate the boiling point of a solution made of 8.59g of ammonium chloride (NHCl) dissolved in 150. g of X. Round you answer to 5 significant digits. пос x10 X

Substance Formula Acetone. lodine Biphenyl C₂H₂O 1₂ C₁₂H₁0 Structure (show all bonds, Aen, label P/NP) Predicted Polarity Solubility Experimentál Solubility Polarity

Dynamic equilibrium can be defined as O rate of dissolution rate of dissolving rate of condensing > rate of bubbling rate of dissolution = rate of recrystallization. rate of dissolution > rate of recrystallization.