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Kennesaw State University *

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Course

3362 LAB

Subject

Chemistry

Date

Dec 6, 2023

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pdf

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1

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ginning of the lab period. Reading Assignment from Zubrick, 9" ed.: Recrystallization pp. 105-113 and the Melting Point Experiment. pp. $8-93; and lodination of Salicylamide, GSU Laboratory Manual 1. Whatiis the purpose for recrystallzing a solid? So we can get the purest form of that sample by removing impurities When you are determ g which solvent you should use for recrystall a Good Solvent” in the Zubrick manual or pant a of the observation(s) are associated with a good recrystallization solvent” A good solvent should work at the boiling point of the solvent but not room temp tion (as in “Finding laboratory exercise) what What information can you get from the melting point of a solid sample? The purity of the sample 4. How much solid should you load into a melting point capillary tube? around 4 mm of solid sample 5. What data is collected for a melting point measurement? The melting point can be used to compare to know compounds S0 we can determine the relative purity of the sample. .
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