A sample of pure water was spiked with 0.520 ng/mL silver ion. Ten replicate determinations of the spiked water sample gave 0.530, 0.510, 0.487, 0.473, 0.514, 0.494, 0.498, 0.502, 0.480, and 0.465 ng/mL silver ion. Determine the mean percent recovery of the spike and the detection limit of the analytical method used for the silver ion determination. mean percent recovery: % detection limit: ng/mL
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- The pH of water samples taken from Iligan Bay was determined. Calculate the pooled estimate of the standard deviation for the analysis, based from the following columns of data: Site No. of Samples measured pH Mean pH Sum of Squares of Deviation from the Mean 1 4 8.02, 8.09, 7.95, 7.98 8.01 0.0110 2 3 7.50, 7.65, 7.49 7.55 0.0161 3 3 8.25, 8.29, 8.20 8.25 0.0041The same chloride analysis but using a new method for which the standard deviation was not known, gave the following replicate results, mean and estimated standard deviation: Chloride (ppm) = 346, 359, 350; Mean = 351.67 ppm; Standard deviation = 6.66ppm. Solve for the CI for the 3 determinations at 95% probability level.In the determination of ethanol concentration in alcoholic beverages using the GCFID method, why do we need to calculate the coefficient variation (CV). standard deviation, repeatability, response factor and response ratio? And how to calculate this parameter?
- A young researcher was evaluating a standard method for determining the methylmercury content in blue fin tuna using high performance liquid chromatography (HPLC). She determined the standard deviation (?)(s) for the method to be 0.440.44 ppb and assumed that ?s was a good approximation of ?σ . As a test, she used this method to evaluate the methylmercury content in a National Institutes of Standards and Technology (NIST) standard and determined the unknown amount to be within 0.210.21 ppb (?)(μ) of the known mean with 99% probability. How many replicate measurements of the NIST standard did the researcher perform?A volume of 250 ml of a 0.05 M solution of a reagent of formula weight (relative molecular mass) 40 was made up, the weighing being done by difference. The standard deviation of each weighing was 0.0001 g: what were the standard deviation and relative standard deviation of the weight of reagent used? The standard deviation of the volume of solvent used was 0.05 ml. Express this as a relative standard deviation. Hence calculate the relative standard deviation of the molarity of the solution. Repeat the calculation for a reagent of formula weight 392.A volume of 250 ml of a 0.05 M solution of a reagent of formula weight (relative molecular mass) 40 was made up, the weighing being done by difference. The standard deviation of each weighing was 0.0001 g. 1 (a) What were the standard deviation and relative standard deviation of the weight of reagent used?
- A volume of 250 ml of a 0.05 M solution of a reagent of formula weight (relative molecular mass) 40 was made up, the weighing being done by difference. The standard deviation of each weighing was 0.0001 g. The standard deviation of the volume of solvent used was 0.05 ml. Express this as a relative standard deviation. Hence calculate the relative standard deviation of the molarity of the solution.FT-IR technique can be utilized for the analysis of unknown analytes by matching it with__________. Both choices are correct Commercial library/database Reference standard25 ml of pickled brine was taken from an apple pickled with vinegar and diluted to 500 ml, 25 ml of this was taken and acidity was determined with 0.2 N (Factor: 1.05) NaOH. In the main trials, 6.3 ml - 6.5 ml - 6.9 ml, respectively, 0.1 ml base was used in the analysis without using the sample.For example, how many ppm is its acidity?
- An analyst determines the Cl^- content of rain water with ion chromatography. The data for the calibration line in the range 5 to 50 milli equivalents per liter (mEq/L) is shown in the table below. Additionally, a blank sample was analysed 5 times and the following results obtained: 1.1, 0.5, 0.1, 0.9 and 1.2 ppm Ct Calculate the detection limit (DL) for the method with a 98.3% confidence level. Use ALL data and show equationsThe ratio of the number of atoms of the isotopes 69Ga and 71Ga in eight samples from different sources was measured in an effort to understand differences in reported values of the atomic mass of gallium: Sample 69Ga/71Ga Sample 69Ga/71Ga1 1.526 60 5 1.528 942 1.529 74 6 1.528 043 1.525 92 7 1.526 854 1.527 31 8 1.527 93 Find the (a) mean, (b) standard deviation, (c) variance, and (d) stan-dard deviation of the mean. (e) Write the mean and standard deviation together with an appropriate number of significant digitsA 0.1475-M solution of Ba(OH)2 was used to titrate the acetic acid (60.05 g/mol) in a dilute aqueous solution. The following results were obtained. (See attached image)(a) Calculate the mean w/v percentage of acetic acid in the sample.(b) Calculate the standard deviation for the results. (Take note if n-1 should be used)(c) Calculate the 90% confidence interval for the mean.(d) (d) At the 90% confidence level, could any of the results be discarded?