A 10 ml of ascorbic acid (MW=176.1) injection was transferred to a 100 ml volumetric flask and made up to volume with deionized water. A 20 ml of the diluted injection was transferred to a conical flask and titrated with Iodine VS using starch mucilage as the indicator. The iodine solution was standardized against a solution of sodium thiosulfate primary standard (MW=248.2).   Results: Weight of sodium thiosulfate used to prepare 100 mL primary standard solution = 2.501 g Volume of thiosulfate solution required to titrate 25 mL of Iodine solution = 24.83 mL Volume of iodine solution required to titrate 20 mL of the diluted ascorbic acid injection = 21.55 mL Stated content of the injection = 10% w/v   Calculate the % of the stated content in the injection. (Round-off your answer to 2-decimal places) Answer = ____%

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter15: Molecular Luminescence Spectrometry
Section: Chapter Questions
Problem 15.7QAP
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A 10 ml of ascorbic acid (MW=176.1) injection was transferred to a 100 ml volumetric flask and made up to volume with deionized water. A 20 ml of the diluted injection was transferred to a conical flask and titrated with Iodine VS using starch mucilage as the indicator. The iodine solution was standardized against a solution of sodium thiosulfate primary standard (MW=248.2).

 

Results:

Weight of sodium thiosulfate used to prepare 100 mL primary standard solution = 2.501 g

Volume of thiosulfate solution required to titrate 25 mL of Iodine solution = 24.83 mL

Volume of iodine solution required to titrate 20 mL of the diluted ascorbic acid injection = 21.55 mL

Stated content of the injection = 10% w/v

 

Calculate the % of the stated content in the injection. (Round-off your answer to 2-decimal places)

Answer = ____%

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