REAGENTS Metallic copper, Concentrated nitric acid, NaOH concentration 6M (25%), Sulfuric acid concentration 3M, Zn shot, 0.1M potassium hydroxide PROCEDURE 1 Weigh out the metallic Cu and place it in a 250mL Erlenmeyer flask. Place the flask near the window and slowly and carefully add concentrated nitric acid. After adding the acid and when the gas begins to evolve, cover the flask with the gas trap stopper and allow the gas to drain into the KOH solution. When the gas stops coming out, and if all the copper is still not dissolved, add more nitric acid and repeat the operations until the Cu dissolves completely. NO2 is released, which is a very toxic reddish-brown gas, so it is important to "catch" it. Write the balanced equation for the reaction between copper and nitric acid. This is an oxide-reduction reaction. Identify the oxidizing and reducing species in the reagents.

Principles of Instrumental Analysis
7th Edition
ISBN:9781305577213
Author:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Chapter33: Automated Methods Of Analysis
Section: Chapter Questions
Problem 33.8QAP
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REAGENTS
Metallic copper, Concentrated nitric acid, NaOH concentration 6M (25%), Sulfuric acid concentration 3M, Zn shot, 0.1M potassium hydroxide

PROCEDURE 1

Weigh out the metallic Cu and place it in a 250mL Erlenmeyer flask. Place the flask near the window and slowly and carefully add concentrated nitric acid. After adding the acid and when the gas begins to evolve, cover the flask with the gas trap stopper and allow the gas to drain into the KOH solution. When the gas stops coming out, and if all the copper is still not dissolved, add more nitric acid and repeat the operations until the Cu dissolves completely. NO2 is released, which is a very toxic reddish-brown gas, so it is important to "catch" it.

Write the balanced equation for the reaction between copper and nitric acid. This is an oxide-reduction reaction. Identify the oxidizing and reducing species in the reagents.

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