A graduate student synthesized the complex [Ir(Cp)(bpy)F](CIO4) using the hydroxide ligand precursor [Ir(Cp)(bpy)(OH)](CIO4). Using your knowledge of XRD, CHN analysis, Mass Spec, vibrational spectroscopy, and NMR, describe how each technique might be used to characterize the product to ensure that no reactant was remaining (i.e. how might each technique differentiate the two molecules?). Give detailed responses on what information would and wouldn't be obtained from each technique.

A graduate student synthesized the complex [Ir(Cp)(bpy)F](CIO4) using the hydroxide ligand precursor [Ir(Cp)(bpy)(OH)](CIO4). Using your knowledge of XRD, CHN analysis, Mass Spec, vibrational spectroscopy, and NMR, describe how each technique might be used to characterize the product to ensure that no reactant was remaining (i.e. how might each technique differentiate the two molecules?). Give detailed responses on what information would and wouldn't be obtained from each technique.

Chemistry

10th Edition

ISBN:9781305957404

Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste

Chapter1: Chemical Foundations

Section: Chapter Questions

Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...

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