EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
expand_more
expand_more
format_list_bulleted
Question
Chapter 10.7, Problem 2E
Interpretation Introduction
Interpretation:The manner yield of
Concept introduction:In order to recover the complete product from it works up solution the excess solvents are removed at a vacuum suction pump. For this purpose Erlenmeyer flask that contains the desired product along with other solvents is placed over the suction pump and is subjected to vacuum as shown in the apparatus below.
Expert Solution & Answer
Want to see the full answer?
Check out a sample textbook solutionStudents have asked these similar questions
write the equations for all chemical reactions that occurred during the extraction process is the Friedel-Crafts Acylation: Synthesis of 4-methoxyacetophenone from anisole experiment :
Include a paragraph to describe the procedure (synthesis of dibenzalacetone) Make sure to discuss the role of the reactants below in the experiment.
Sodium hydroxide
Ethyl alcohol
Acetone
Benzaldehyde
In a benzopinacolone synthesis, if the crude product obtained at the end of the reaction has a brown color (brown-violet), why is this possible? How could this be avoided?
Chapter 10 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
Ch. 10.2 - Prob. 1ECh. 10.2 - Prob. 2ECh. 10.2 - Prob. 3ECh. 10.2 - Prob. 4ECh. 10.2 - Prob. 5ECh. 10.2 - Prob. 6ECh. 10.2 - Prob. 7ECh. 10.2 - Prob. 8ECh. 10.2 - Prob. 9ECh. 10.2 - Prob. 10E
Ch. 10.2 - Prob. 11ECh. 10.2 - Prob. 12ECh. 10.2 - Prob. 13ECh. 10.2 - Prob. 14ECh. 10.2 - Prob. 15ECh. 10.2 - Prob. 16ECh. 10.2 - Prob. 17ECh. 10.3 - Prob. 1ECh. 10.3 - Prob. 2ECh. 10.3 - Prob. 3ECh. 10.3 - Prob. 4ECh. 10.3 - Prob. 5ECh. 10.3 - Prob. 6ECh. 10.3 - Prob. 7ECh. 10.3 - Prob. 8ECh. 10.3 - Prob. 9ECh. 10.3 - Prob. 10ECh. 10.3 - Prob. 11ECh. 10.3 - Prob. 12ECh. 10.3 - Prob. 13ECh. 10.3 - Prob. 14ECh. 10.3 - Prob. 15ECh. 10.3 - Prob. 16ECh. 10.3 - Prob. 17ECh. 10.3 - Prob. 18ECh. 10.3 - Prob. 19ECh. 10.3 - Prob. 20ECh. 10.3 - Prob. 21ECh. 10.3 - Prob. 22ECh. 10.3 - Prob. 23ECh. 10.3 - Prob. 24ECh. 10.3 - Prob. 25ECh. 10.3 - Prob. 26ECh. 10.3 - Prob. 27ECh. 10.3 - Prob. 28ECh. 10.3 - Prob. 29ECh. 10.3 - Prob. 30ECh. 10.3 - Prob. 31ECh. 10.3 - Prob. 32ECh. 10.5 - Prob. 1ECh. 10.5 - Prob. 2ECh. 10.5 - Prob. 3ECh. 10.5 - Prob. 4ECh. 10.5 - Prob. 5ECh. 10.5 - Prob. 6ECh. 10.5 - Prob. 7ECh. 10.5 - Prob. 8ECh. 10.5 - Prob. 9ECh. 10.5 - Prob. 10ECh. 10.5 - Prob. 11ECh. 10.5 - Prob. 12ECh. 10.5 - Prob. 14ECh. 10.5 - Prob. 15ECh. 10.5 - Prob. 16ECh. 10.5 - Prob. 17ECh. 10.5 - Prob. 18ECh. 10.5 - Prob. 19ECh. 10.5 - Prob. 20ECh. 10.5 - Prob. 23ECh. 10.6 - Prob. 1ECh. 10.6 - Prob. 2ECh. 10.6 - Prob. 3ECh. 10.6 - Prob. 4ECh. 10.6 - Prob. 5ECh. 10.6 - Prob. 6ECh. 10.6 - Prob. 7ECh. 10.6 - Prob. 8ECh. 10.6 - Prob. 9ECh. 10.6 - Prob. 10ECh. 10.6 - Prob. 11ECh. 10.6 - Prob. 12ECh. 10.6 - Prob. 13ECh. 10.6 - Prob. 14ECh. 10.6 - Prob. 15ECh. 10.6 - Prob. 16ECh. 10.6 - Prob. 17ECh. 10.6 - Prob. 18ECh. 10.6 - Prob. 20ECh. 10.6 - Prob. 21ECh. 10.6 - Prob. 22ECh. 10.6 - Prob. 23ECh. 10.6 - Prob. 24ECh. 10.6 - Prob. 25ECh. 10.6 - Prob. 26ECh. 10.6 - Prob. 28ECh. 10.6 - Prob. 29ECh. 10.6 - Prob. 30ECh. 10.7 - Prob. 1ECh. 10.7 - Prob. 2ECh. 10.7 - Prob. 3ECh. 10.7 - Prob. 4ECh. 10.7 - Prob. 5ECh. 10.7 - Prob. 6ECh. 10.7 - Prob. 7ECh. 10.7 - Prob. 8ECh. 10.7 - Prob. 9ECh. 10.7 - Prob. 10ECh. 10.7 - Prob. 11ECh. 10.7 - Prob. 12ECh. 10.8 - Prob. 1ECh. 10.8 - Prob. 2ECh. 10.8 - Prob. 4ECh. 10.8 - Prob. 5ECh. 10.8 - Prob. 6ECh. 10.8 - Prob. 7ECh. 10.8 - Prob. 8ECh. 10.8 - Prob. 9ECh. 10.8 - Prob. 10ECh. 10.8 - Prob. 11ECh. 10.8 - Prob. 12ECh. 10.8 - Prob. 13ECh. 10.8 - Prob. 14ECh. 10.8 - Prob. 15E
Knowledge Booster
Similar questions
- 1. Why does p-nitroacetanilide recrystallize in ethanol, but the o-acetanilide remains in the filtrate? 2. Give two reasons why a water bath can and must be used during the recrystallisation of benzoin synthesisis.arrow_forwardwhat is prefromulation steps of phenylbutazone ?with illustration?arrow_forwardExplain how you would proceed to isolate (R)-(+)-α-phenylethylamine from the mother liquor that remained after you crystallized (S)-(-)-α-phenylethylamine.arrow_forward
- Briefly describe the process of Fischer esterification of methyl salicylate.arrow_forwardGive an inference and observation when the compound hexane is subjected into Tollen's test and Iodoform Testarrow_forwardWhy does p-nitroacetanilide recrystallize in ethanol, but the o-acetanilide remains in the filtrate during amide synthesis( the synthesis of p-nitroacetanilide).arrow_forward
- Diethylacetal can be detected by gas chromatography. How does this impurity arise in fermentation?arrow_forwardA mixture containing compounds A and B in methylene chloride (CH2Cl2) was extracted in a separatory funnel containing aqueous HCl. Which compound migrates to the aqueous layer? Why?arrow_forwardWhat would be the equation for the chemcical reaction of 4-acetylbenzaldehyde in the iodoform test? Thank you!arrow_forward
- In a few sentences, briefly explain the difference between acid catalyzed and base promoted enolation of aldehydes and ketones.arrow_forwardHow do you deprotect the side-chain carboxyl under mild conditions without removing the BOC-protecting group at the same time?arrow_forwardWhat is the reaction mechanism for the conversion of acetophenone to its corresponding alpha,beta-unsaturated ester using the product of the Arbuzov reaction under Horner-Wadsworth-Emmons reaction conditions?arrow_forward
arrow_back_ios
SEE MORE QUESTIONS
arrow_forward_ios
Recommended textbooks for you
- Macroscale and Microscale Organic ExperimentsChemistryISBN:9781305577190Author:Kenneth L. Williamson, Katherine M. MastersPublisher:Brooks ColeOrganic ChemistryChemistryISBN:9781305580350Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. FootePublisher:Cengage Learning
Macroscale and Microscale Organic Experiments
Chemistry
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Brooks Cole
Organic Chemistry
Chemistry
ISBN:9781305580350
Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote
Publisher:Cengage Learning